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Selection of catalyst and reaction conditions for ultrasound assisted biodiesel production from canola oil

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  • Korkut, Ibrahim
  • Bayramoglu, Mahmut

Abstract

In this study, the experimental optimization of ultrasound assisted biodiesel production in presence of heterogeneous catalyst was investigated. Three catalysts namely; CaO, calcined dolomite and calcium diglyceroxide (CaDG) were taken into account for comparative purpose. D-optimal experimental plan was applied to obtain regression models which were subsequently used for the detection of optimum process conditions. Maximum biodiesel yields were calculated as 98.7%, 95.9% and 86.3% for CaO, calcined dolomite and CaDG respectively. Furthermore, supplemental experiments were conducted around optimum process conditions to test the validity of the regression models and to refine the optimum results. Finally, in the case of CaO catalyst, maximum biodiesel yield (99.4%) was obtained at the following conditions; catalyst loading: 5.35% (wt.of oil), methanol/oil ratio: 7.48, ultrasonic power: 40 W, time: 150 min, and reaction temperature: 60 °C.

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  • Korkut, Ibrahim & Bayramoglu, Mahmut, 2018. "Selection of catalyst and reaction conditions for ultrasound assisted biodiesel production from canola oil," Renewable Energy, Elsevier, vol. 116(PA), pages 543-551.
    • Handle: RePEc:eee:renene:v:116:y:2018:i:pa:p:543-551
    DOI: 10.1016/j.renene.2017.10.010
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    1. Marinković, Dalibor M. & Stanković, Miroslav V. & Veličković, Ana V. & Avramović, Jelena M. & Miladinović, Marija R. & Stamenković, Olivera O. & Veljković, Vlada B. & Jovanović, Dušan M., 2016. "Calcium oxide as a promising heterogeneous catalyst for biodiesel production: Current state and perspectives," Renewable and Sustainable Energy Reviews, Elsevier, vol. 56(C), pages 1387-1408.
    2. Chouhan, A.P. Singh & Sarma, A.K., 2011. "Modern heterogeneous catalysts for biodiesel production: A comprehensive review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 15(9), pages 4378-4399.
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    2. Shelare, Sagar D. & Belkhode, Pramod N. & Nikam, Keval Chandrakant & Jathar, Laxmikant D. & Shahapurkar, Kiran & Soudagar, Manzoore Elahi M. & Veza, Ibham & Khan, T.M. Yunus & Kalam, M.A. & Nizami, Ab, 2023. "Biofuels for a sustainable future: Examining the role of nano-additives, economics, policy, internet of things, artificial intelligence and machine learning technology in biodiesel production," Energy, Elsevier, vol. 282(C).
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    6. Silitonga, A.S. & Mahlia, T.M.I. & Kusumo, F. & Dharma, S. & Sebayang, A.H. & Sembiring, R.W. & Shamsuddin, A.H., 2019. "Intensification of Reutealis trisperma biodiesel production using infrared radiation: Simulation, optimisation and validation," Renewable Energy, Elsevier, vol. 133(C), pages 520-527.
    7. Pascoal, C.V.P. & Oliveira, A.L.L. & Figueiredo, D.D. & Assunção, J.C.C., 2020. "Optimization and kinetic study of ultrasonic-mediated in situ transesterification for biodiesel production from the almonds of Syagrus cearensis," Renewable Energy, Elsevier, vol. 147(P1), pages 1815-1824.
    8. Oza, Suvik & Kodgire, Pravin & Kachhwaha, Surendra Singh & Lam, Man Kee & Yusup, Suzana & Chai, Yee Ho & Rokhum, Samuel Lalthazuala, 2024. "A review on sustainable and scalable biodiesel production using ultra-sonication technology," Renewable Energy, Elsevier, vol. 226(C).

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