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Thermal Decomposition of Olive-Mill Byproducts: A TG-FTIR Approach

Author

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  • Małgorzata Wzorek

    (Department of Process and Environmental Engineering, Faculty of Mechanical Engineering, Opole University of Technology, 5 Mikołajczyka Str., 45-271 Opole, Poland)

  • Robert Junga

    (Department of Thermal Engineering and Industrial Facilities, Faculty of Mechanical Engineering, Opole University of Technology, 5 Mikołajczyka Str., 45-271 Opole, Poland)

  • Ersel Yilmaz

    (Department of Biosystems Engineering, Faculty of Agriculture, Adnan Menderes University, Aydin 09020, Turkey)

  • Bohdan Bozhenko

    (Department of Mathematics and IT Applications, Faculty of Production Engineering and Logistics, Opole University of Technology, 31 Sosnkowskiego Str., 45-271 Opole, Poland)

Abstract

In this study, the combustion of olive byproducts was investigated using the TG-FTIR technique. Different types of olive biomass were considered: twigs, leaves, olive-mill waste from the two-phase decanting method, and wastewater from the three-phase system. The reaction regions, ignition, and burnout temperatures at different heating rates were determined using TG/DTG analysis and the thermogravimetry results. Comprehensive combustion, ignition, burnout, and flammability indexes were also calculated. The highest combustion index values were obtained for waste from the three-phase system, followed by the two-phase decanting method, then with leaves and small twigs. The order of the index values indicated that the sample from the three-phase process ignited more quickly and yielded faster. The changes in activation energy calculated using different model-free isoconversional methods—Friedman, Ozawa–Flynn–Wall, and Kissinger–Akahira–Sunose—fell within the range of 130–140 kJ/kmol. FTIR analyses presented differences in the exhaust gas composition for specific combustion temperature ranges.

Suggested Citation

  • Małgorzata Wzorek & Robert Junga & Ersel Yilmaz & Bohdan Bozhenko, 2021. "Thermal Decomposition of Olive-Mill Byproducts: A TG-FTIR Approach," Energies, MDPI, vol. 14(14), pages 1-16, July.
    • Handle: RePEc:gam:jeners:v:14:y:2021:i:14:p:4123-:d:590839
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    References listed on IDEAS

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    Cited by:

    1. Biagio Morrone, 2022. "Residual Biomass Conversion to Bioenergy," Energies, MDPI, vol. 15(16), pages 1-3, August.

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