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In Deep Analysis on the Behavior of Grape Marc Constituents during Hydrothermal Carbonization

Author

Listed:
  • Daniele Basso

    (Faculty of Science and Technology, Free University of Bolzano, Piazza Università 5, 39100 Bolzano, Italy)

  • Elsa Weiss-Hortala

    (IMT Mines Albi, Centre RAPSODEE, UMR CNRS 5302, Campus Jarlard, F-81013 Albi CEDEX 09, France)

  • Francesco Patuzzi

    (Faculty of Science and Technology, Free University of Bolzano, Piazza Università 5, 39100 Bolzano, Italy)

  • Marco Baratieri

    (Faculty of Science and Technology, Free University of Bolzano, Piazza Università 5, 39100 Bolzano, Italy)

  • Luca Fiori

    (DICAM, Department of Civil, Environmental and Mechanical Engineering, University of Trento—Via Mesiano 77, 38123 Trento, Italy)

Abstract

Grape marc is a residue of the wine-making industry, nowadays not always effectively valorized. It consists of grape seeds (mostly lignocellulosic) and grape skins (mostly holocellulosic). In order to understand possible correlations between seeds and skins in forming hydrochar for it to be used as a solid biofuel, hydrothermal carbonization (HTC) was applied separately to grape marc and its constituents. HTC was performed at several process conditions (temperature: 180, 220 and 250 °C; reaction time: 0.5, 1, 3 and 8 h), in order to collect data on the three phases formed downstream of the process: solid (hydrochar), liquid and gas. An in deep analytical characterization was performed: ultimate analysis and calorific value for hydrochar, Total Organic Carbon (TOC) and Inductively Coupled Plasma (IPC) analyses for liquid phase, composition for gas phase. In previous works, the same experimental apparatus was used to treat residual biomass, obtaining interesting results in terms of possible hydrochar exploitation as a solid biofuel. Thus, the main objectives of this work were both to get results for validating the hypothesis to apply HTC to this feedstock, and to collect data for subsequent theoretical investigations. Moreover, a severity model was developed to allow a predictive description of the hydrochar yield as a function of a unique parameter condensing both temperature and reaction time effects. The results obtained demonstrate that this process can upgrade wet residues into a solid biofuel ad that the process can be satisfactorily described in terms of a severity factor.

Suggested Citation

  • Daniele Basso & Elsa Weiss-Hortala & Francesco Patuzzi & Marco Baratieri & Luca Fiori, 2018. "In Deep Analysis on the Behavior of Grape Marc Constituents during Hydrothermal Carbonization," Energies, MDPI, vol. 11(6), pages 1-19, May.
    • Handle: RePEc:gam:jeners:v:11:y:2018:i:6:p:1379-:d:149488
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    References listed on IDEAS

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    1. Michela Lucian & Luca Fiori, 2017. "Hydrothermal Carbonization of Waste Biomass: Process Design, Modeling, Energy Efficiency and Cost Analysis," Energies, MDPI, vol. 10(2), pages 1-18, February.
    2. Xing Yang & Hailong Wang & Peter James Strong & Song Xu & Shujuan Liu & Kouping Lu & Kuichuan Sheng & Jia Guo & Lei Che & Lizhi He & Yong Sik Ok & Guodong Yuan & Ying Shen & Xin Chen, 2017. "Thermal Properties of Biochars Derived from Waste Biomass Generated by Agricultural and Forestry Sectors," Energies, MDPI, vol. 10(4), pages 1-12, April.
    3. Lu, Liang & Namioka, Tomoaki & Yoshikawa, Kunio, 2011. "Effects of hydrothermal treatment on characteristics and combustion behaviors of municipal solid wastes," Applied Energy, Elsevier, vol. 88(11), pages 3659-3664.
    4. Seung-Yong Oh & Young-Man Yoon, 2017. "Energy Recovery Efficiency of Poultry Slaughterhouse Sludge Cake by Hydrothermal Carbonization," Energies, MDPI, vol. 10(11), pages 1-13, November.
    5. Shi-Xiang Zhao & Na Ta & Xu-Dong Wang, 2017. "Effect of Temperature on the Structural and Physicochemical Properties of Biochar with Apple Tree Branches as Feedstock Material," Energies, MDPI, vol. 10(9), pages 1-15, August.
    6. Chamseddine Guizani & Mejdi Jeguirim & Sylvie Valin & Lionel Limousy & Sylvain Salvador, 2017. "Biomass Chars: The Effects of Pyrolysis Conditions on Their Morphology, Structure, Chemical Properties and Reactivity," Energies, MDPI, vol. 10(6), pages 1-18, June.
    7. Chang Liu & Xin Huang & Lingzhao Kong, 2017. "Efficient Low Temperature Hydrothermal Carbonization of Chinese Reed for Biochar with High Energy Density," Energies, MDPI, vol. 10(12), pages 1-10, December.
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    Cited by:

    1. Nepu Saha & Maurizio Volpe & Luca Fiori & Roberto Volpe & Antonio Messineo & M. Toufiq Reza, 2020. "Cationic Dye Adsorption on Hydrochars of Winery and Citrus Juice Industries Residues: Performance, Mechanism, and Thermodynamics," Energies, MDPI, vol. 13(18), pages 1-16, September.
    2. Ramos, João S. & Ferreira, Ana F., 2022. "Techno-economic analysis and life cycle assessment of olive and wine industry co-products valorisation," Renewable and Sustainable Energy Reviews, Elsevier, vol. 155(C).
    3. Isaac Lorero & Arturo J. Vizcaíno & Francisco J. Alguacil & Félix A. López, 2020. "Activated Carbon from Winemaking Waste: Thermoeconomic Analysis for Large-Scale Production," Energies, MDPI, vol. 13(23), pages 1-22, December.
    4. René A. Garrido & Camila Lagos & Carolina Luna & Jaime Sánchez & Georgina Díaz, 2021. "Study of the Potential Uses of Hydrochar from Grape Pomace and Walnut Shells Generated from Hydrothermal Carbonization as an Alternative for the Revalorization of Agri-Waste in Chile," Sustainability, MDPI, vol. 13(22), pages 1-10, November.
    5. Roberta Ferrentino & Fabio Merzari & Luca Fiori & Gianni Andreottola, 2020. "Coupling Hydrothermal Carbonization with Anaerobic Digestion for Sewage Sludge Treatment: Influence of HTC Liquor and Hydrochar on Biomethane Production," Energies, MDPI, vol. 13(23), pages 1-19, November.
    6. Md Tahmid Islam & Al Ibtida Sultana & Cadianne Chambers & Swarna Saha & Nepu Saha & Kawnish Kirtania & M. Toufiq Reza, 2022. "Recent Progress on Emerging Applications of Hydrochar," Energies, MDPI, vol. 15(24), pages 1-45, December.

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