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Valorization of hazard waste: Efficient utilization of white brick waste powder in the catalytic production of biodiesel from waste cooking oil via RSM optimization process

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  • Abu-Ghazala, Abdelmoniem H.
  • Abdelhady, Hosam H.
  • Mazhar, Amina A.
  • El-Deab, Mohamed S.

Abstract

The target of this study is to utilize hazardous white brick waste powder as a heterogeneous catalyst for biodiesel production through the transesterification process of waste cooking oil (WCO) and methanol. Physico-chemical characterization of the processed waste has been carried out using various techniques including TGA, XRD, FT-IR, BET surface area, FE-SEM & mapping EDX, XRF, and CO2-TPD. The influence of calcination temperature on the catalytic activity is studied. The optimization process of variable independent parameters i.e., catalyst loading, reaction temperature and time as well as alcohol:WCO molar ratio is performed via response surface methodology (RSM) through central composite design (CCD). Optimum conditions (biodiesel conversion = 92.7%) are: catalyst loading 1.3%; temperature 64 °C; methanol:WCO molar ratio of 5.5:1; and reaction time 139 min. Kinetic parameters, i.e., rate constant (k), activation energy (Ea = 25.95 kJ/mol) and thermodynamic parameters, i.e., ΔS# and ΔH# of −202.36 J/mol and +23.27 kJ/mol, respectively, are estimated. The reusability of the prepared catalyst is performed up to six consecutives cycles with marginal loss in activity. Physico-chemical properties of the prepared biodiesel are comparable with the ASTM D-6751 and EN-14214 standard ranges.

Suggested Citation

  • Abu-Ghazala, Abdelmoniem H. & Abdelhady, Hosam H. & Mazhar, Amina A. & El-Deab, Mohamed S., 2022. "Valorization of hazard waste: Efficient utilization of white brick waste powder in the catalytic production of biodiesel from waste cooking oil via RSM optimization process," Renewable Energy, Elsevier, vol. 200(C), pages 1120-1133.
    • Handle: RePEc:eee:renene:v:200:y:2022:i:c:p:1120-1133
    DOI: 10.1016/j.renene.2022.10.045
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