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Evaluation of oxidative stability of soybean biodiesel using ethanolic and chloroform extracts of Platymiscium floribundum as antioxidant

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  • Nogueira, Tiago Rocha
  • de Mesquita Figueredo, Igor
  • Tavares Luna, Francisco Murilo
  • Cavalcante, Célio Loureiro
  • Evangelista de Ávila dos Santos, João
  • Sousa Lima, Mary Anne
  • Josino da Silva, Thiala Soares
  • Almeida Moreira Leal, Luzia Kalyne
  • Nunes, Fátima Miranda
  • Alexsandra de Sousa Rios, Maria
  • Ávila Pimenta, Antônia Torres

Abstract

The objective of this work was to evaluate the effect of Platymiscium floribundum ethanolic and chloroform extracts on the oxidative stability of soybean biodiesel using the Rancimat and DSC methods. The soybean biodiesel was obtained by transesterification. The antioxidant activity of the extracts was also evaluated by the free radical scavenging (DPPH) method and the total phenolic content by the Folin-Ciocalteu method. Both extracts showed antioxidant activity, reducing the DPPH by about 90%, and the total phenolic content of the ethanolic and chloroform extracts were 2.87 and 3.10 mg GAE/100 mg of extract, respectively. The extracts showed to be very efficient in retarding the oxidation of soybean biodiesel since the induction period increased from 4.53 h to 18.09 h (PF–EtOH, 10000 mg/kg) and 17.58 h (PF–CHCl3, 10000 mg/kg). Both extracts showed high thermal stability with Ton-e of 405.76 °C (PF–CHCl3) and 396.79 °C (PF–EtOH). The presence of the extracts increased the activation energy of the samples between 12.3% and 37.0%. The increase of the activation energy represents an improvement of the oxidative stability of biodiesel. All results confirmed the action of the antioxidants present in the extracts on controlling the oxidation reactions in biodiesel.

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  • Nogueira, Tiago Rocha & de Mesquita Figueredo, Igor & Tavares Luna, Francisco Murilo & Cavalcante, Célio Loureiro & Evangelista de Ávila dos Santos, João & Sousa Lima, Mary Anne & Josino da Silva, Thi, 2020. "Evaluation of oxidative stability of soybean biodiesel using ethanolic and chloroform extracts of Platymiscium floribundum as antioxidant," Renewable Energy, Elsevier, vol. 159(C), pages 767-774.
    • Handle: RePEc:eee:renene:v:159:y:2020:i:c:p:767-774
    DOI: 10.1016/j.renene.2020.06.062
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    1. Sander, Aleksandra & Antonije Košćak, Mihael & Kosir, Dominik & Milosavljević, Nikola & Parlov Vuković, Jelena & Magić, Lana, 2018. "The influence of animal fat type and purification conditions on biodiesel quality," Renewable Energy, Elsevier, vol. 118(C), pages 752-760.
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    1. Zhang, Xiaokang & Li, Nana & Wei, Zhong & Dai, Bin & Han, Sheng, 2022. "Synthesis and evaluation of bifunctional polymeric agent for improving cold flow properties and oxidation stability of diesel-biodiesel blends," Renewable Energy, Elsevier, vol. 196(C), pages 737-748.
    2. Umar, Yusuf & Velasco, Orlando & Abdelaziz, Omar Y. & Aboelazayem, Omar & Gadalla, Mamdouh A. & Hulteberg, Christian P. & Saha, Basudeb, 2022. "A renewable lignin-derived bio-oil for boosting the oxidation stability of biodiesel," Renewable Energy, Elsevier, vol. 182(C), pages 867-878.

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