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CO2 capture performance of synthetic sorbent prepared from carbide slag and aluminum nitrate hydrate by combustion synthesis

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  • Li, Yingjie
  • Su, Mengying
  • Xie, Xin
  • Wu, Shuimu
  • Liu, Changtian

Abstract

A new CO2 sorbent was prepared from carbide slag, aluminum nitrate hydrate and glycerol water solution by combustion synthesis method. The effects of the sorbent preparation conditions (glycerol addition, combustion synthesis temperature, ratio of carbide slag to aluminum nitrate hydrate) and carbonation/calcination conditions (temperature, atmosphere and time) on CO2 capture performance of the synthetic sorbent were investigated in the calcium looping cycles. The addition of glycerol during the sorbent preparation exhibits an improvement on the cyclic CO2 capture capacity. It was also found that the optimal combustion synthesis temperature for the synthetic sorbent was in the range of 750–800°C. The synthetic sorbent contained the mass ratio of CaO derived from carbide slag to Al2O3 derived from aluminum nitrate hydrate=90:10 exhibited higher CO2 capture capacity (0.38g CO2/g sorbent after 50cycles). X-ray diffraction analysis showed that the main compounds of the synthetic sorbent were CaO and Ca3Al2O6 by X-ray diffraction analysis. The synthetic sorbent showed higher CO2 capture capacity than the carbide slag under severe calcination conditions (950°C, CO2) and at short carbonation time (<5min). From the present investigation, it shows that a high active synthetic CO2 sorbent could be obtained using the carbide slag in the calcium looping technology.

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  • Li, Yingjie & Su, Mengying & Xie, Xin & Wu, Shuimu & Liu, Changtian, 2015. "CO2 capture performance of synthetic sorbent prepared from carbide slag and aluminum nitrate hydrate by combustion synthesis," Applied Energy, Elsevier, vol. 145(C), pages 60-68.
  • Handle: RePEc:eee:appene:v:145:y:2015:i:c:p:60-68
    DOI: 10.1016/j.apenergy.2015.01.061
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    7. Hong-Hua Qiu & Lu-Ge Liu, 2018. "A Study on the Evolution of Carbon Capture and Storage Technology Based on Knowledge Mapping," Energies, MDPI, vol. 11(5), pages 1-25, May.
    8. Li, Caili & Li, Yingjie & Fang, Yi & Zhang, Chunxiao & Ren, Yu, 2024. "TiO2/MnFe2O4 co-modified alkaline papermaking waste for CaO-CaCO3 thermochemical energy storage," Applied Energy, Elsevier, vol. 362(C).
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    10. Zhang, Jianan & Wang, Yuesen & Muldoon, Valerie L. & Deng, Sili, 2022. "Crude glycerol and glycerol as fuels and fuel additives in combustion applications," Renewable and Sustainable Energy Reviews, Elsevier, vol. 159(C).
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    12. Su, Chenglin & Duan, Lunbo & Donat, Felix & Anthony, Edward John, 2018. "From waste to high value utilization of spent bleaching clay in synthesizing high-performance calcium-based sorbent for CO2 capture," Applied Energy, Elsevier, vol. 210(C), pages 117-126.
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    14. Xiaotong Ma & Yingjie Li & Yi Qian & Zeyan Wang, 2019. "A Carbide Slag-Based, Ca 12 Al 14 O 33 -Stabilized Sorbent Prepared by the Hydrothermal Template Method Enabling Efficient CO 2 Capture," Energies, MDPI, vol. 12(13), pages 1-17, July.
    15. Jing, Jie-ying & Li, Ting-yu & Zhang, Xue-wei & Wang, Shi-dong & Feng, Jie & Turmel, William A. & Li, Wen-ying, 2017. "Enhanced CO2 sorption performance of CaO/Ca3Al2O6 sorbents and its sintering-resistance mechanism," Applied Energy, Elsevier, vol. 199(C), pages 225-233.
    16. Gong, Xuzhong & Zhang, Tong & Zhang, Junqiang & Wang, Zhi & Liu, Junhao & Cao, Jianwei & Wang, Chuan, 2022. "Recycling and utilization of calcium carbide slag - current status and new opportunities," Renewable and Sustainable Energy Reviews, Elsevier, vol. 159(C).
    17. Laixing Luo & Xing Zheng & Jianye Wang & Wu Qin & Xianbin Xiao & Zongming Zheng, 2021. "Catalyzed Ethanol Chemical Looping Gasification Mechanism on the Perfect and Reduced Fe 2 O 3 Surfaces," Energies, MDPI, vol. 14(6), pages 1-15, March.
    18. Shi, Jiewen & Li, Yingjie & Zhang, Qing & Ma, Xiaotong & Duan, Lunbo & Zhou, Xingang, 2017. "CO2 capture performance of a novel synthetic CaO/sepiolite sorbent at calcium looping conditions," Applied Energy, Elsevier, vol. 203(C), pages 412-421.
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    20. Zhang, Wan & Li, Yingjie & He, Zirui & Ma, Xiaotong & Song, Haiping, 2017. "CO2 capture by carbide slag calcined under high-concentration steam and energy requirement in calcium looping conditions," Applied Energy, Elsevier, vol. 206(C), pages 869-878.

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