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Influences of hydrochloric acid washing on the thermal decomposition behavior and thermodynamic parameters of sweet sorghum stalk

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  • Chen, Dongyu
  • Gao, Dongxiao
  • Capareda, Sergio C.
  • E, Shuang
  • Jia, Fengrui
  • Wang, Ying

Abstract

The influences of hydrochloric acid washing on the pyrolysis behavior and thermodynamic parameters of sweet sorghum stalk were investigated using thermogravimetric analysis and Fourier transform infrared (FTIR) in this study. Hydrochloric acid washing influenced the quality of sweet sorghum stalk and changed the pyrolysis curves shape. By acid pretreatment, the 98% of metals and 47.15% of extractives were removed, the maximum weight loss rates were improved by 1.53–1.64 times, the volatiles yields were enhanced about 10%, and the high heat value increased from 15.59 to 18.27 MJ/kg. Lower activation energies were obtained for acid-washed samples at conversion rate >0.45 by the Flynn-Wall-Ozawa and Kissinger-Akahira-Sunose (KAS) methods. The higher Gibbs free energy of 133.94–137.79 kJ/mol could provide more energy for pretreatment samples, and FTIR analysis confirmed acid washing could change functional groups in samples.

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  • Chen, Dongyu & Gao, Dongxiao & Capareda, Sergio C. & E, Shuang & Jia, Fengrui & Wang, Ying, 2020. "Influences of hydrochloric acid washing on the thermal decomposition behavior and thermodynamic parameters of sweet sorghum stalk," Renewable Energy, Elsevier, vol. 148(C), pages 1244-1255.
    • Handle: RePEc:eee:renene:v:148:y:2020:i:c:p:1244-1255
    DOI: 10.1016/j.renene.2019.10.064
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    1. Banerji, Aditi & Balakrishnan, M. & Kishore, V.V.N., 2013. "Low severity dilute-acid hydrolysis of sweet sorghum bagasse," Applied Energy, Elsevier, vol. 104(C), pages 197-206.
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    5. Carvalho, Wender Santana & Santana Júnior, José Alair & de Oliveira, Tiago José Pires & Ataíde, Carlos Henrique, 2017. "Fast pyrolysis of sweet sorghum bagasse in a fluidized bed reactor: Product characterization and comparison with vapors generated in analytical pyrolysis," Energy, Elsevier, vol. 131(C), pages 186-197.
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    1. Liu, Hui & Liu, Jingyong & Huang, Hongyi & Evrendilek, Fatih & Wen, Shaoting & Li, Weixin, 2021. "Optimizing bioenergy and by-product outputs from durian shell pyrolysis," Renewable Energy, Elsevier, vol. 164(C), pages 407-418.
    2. Shulun Han & Li Bai & Mingshu Chi & Xiuling Xu & Zhao Chen & Kecheng Yu, 2022. "Conversion of Waste Corn Straw to Value-Added Fuel via Hydrothermal Carbonization after Acid Washing," Energies, MDPI, vol. 15(5), pages 1-14, March.

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