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Properties of ash generated during sewage sludge combustion: A multifaceted analysis

Author

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  • Magdziarz, Aneta
  • Wilk, Małgorzata
  • Gajek, Marcin
  • Nowak-Woźny, Dorota
  • Kopia, Agnieszka
  • Kalemba-Rec, Izabela
  • Koziński, Janusz A.

Abstract

This paper presents chemical properties of sewage sludge ashes required for determining their thermal characteristics. A novel approach, linking selected advanced analytical techniques with FactSage modelling, was developed and applied to obtain new information on deposit formation mechanisms that contribute to fouling and slagging. The mineral matter and fusion temperatures were investigated using a variety of analytical techniques including XRF, ICP-MS, XRD, SEM-EDX and AFT. The slagging and fouling indices were calculated and the sintering properties were predicted. The studied ashes were rich in P2O5, CaO, SiO2 and Fe2O3, but their concentrations slightly differed. Phase analyses suggested the existence of calcium and phosphorus as main phases. Thermal behaviour of ashes was studied focusing on the mass loss, temperature peaks and thermic effects with the increasing of temperature up to 1200 °C under air atmosphere. The changes in concentration of ash compounds contributed to differences in ash fusion temperatures. FactSage thermochemical equilibrium calculations were used to predict the amount of liquid slag and solid phases, giving information about slagging properties of ashes. The general conclusion based on experimental studies is that sewage sludge ashes cause the slagging and fouling hazard while they reveal low corrosive effect.

Suggested Citation

  • Magdziarz, Aneta & Wilk, Małgorzata & Gajek, Marcin & Nowak-Woźny, Dorota & Kopia, Agnieszka & Kalemba-Rec, Izabela & Koziński, Janusz A., 2016. "Properties of ash generated during sewage sludge combustion: A multifaceted analysis," Energy, Elsevier, vol. 113(C), pages 85-94.
    • Handle: RePEc:eee:energy:v:113:y:2016:i:c:p:85-94
    DOI: 10.1016/j.energy.2016.07.029
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    4. Karol Król & Wojciech Moroń & Dorota Nowak-Woźny, 2022. "Biomass and Coal Ash Sintering—Thermodynamic Equilibrium Modeling versus Pressure Drop Test and Mechanical Test," Energies, MDPI, vol. 16(1), pages 1-16, December.
    5. Zhang, Zhe & Liu, Congmin & Liu, Wei & Du, Xu & Cui, Yong & Gong, Jian & Guo, Hua & Deng, Yulin, 2017. "Direct conversion of sewage sludge to electricity using polyoxomatelate catalyzed flow fuel cell," Energy, Elsevier, vol. 141(C), pages 1019-1026.
    6. Karol Król & Dorota Nowak-Woźny & Wojciech Moroń, 2023. "Study of Ash Sintering Temperature and Ash Deposition Behavior during Co-Firing of Polish Bituminous Coal with Barley Straw Using Non-Standard Tests," Energies, MDPI, vol. 16(11), pages 1-15, May.
    7. Syed-Hassan, Syed Shatir A. & Wang, Yi & Hu, Song & Su, Sheng & Xiang, Jun, 2017. "Thermochemical processing of sewage sludge to energy and fuel: Fundamentals, challenges and considerations," Renewable and Sustainable Energy Reviews, Elsevier, vol. 80(C), pages 888-913.
    8. Magdziarz, Aneta & Gajek, Marcin & Nowak-Woźny, Dorota & Wilk, Małgorzata, 2018. "Mineral phase transformation of biomass ashes – Experimental and thermochemical calculations," Renewable Energy, Elsevier, vol. 128(PB), pages 446-459.
    9. Ilham Gbouri & Fan Yu & Xutong Wang & Junxia Wang & Xiaoqiang Cui & Yanjun Hu & Beibei Yan & Guanyi Chen, 2022. "Co-Pyrolysis of Sewage Sludge and Wetland Biomass Waste for Biochar Production: Behaviors of Phosphorus and Heavy Metals," IJERPH, MDPI, vol. 19(5), pages 1-16, February.
    10. Skrzypczak, Dawid & Trzaska, Krzysztof & Mikula, Katarzyna & Gil, Filip & Izydorczyk, Grzegorz & Mironiuk, Małgorzata & Polomska, Xymena & Moustakas, Konstantinos & Witek-Krowiak, Anna & Chojnacka, Ka, 2023. "Conversion of anaerobic digestates from biogas plants: Laboratory fertilizer formulation, scale-up and demonstration of applicative properties on plants," Renewable Energy, Elsevier, vol. 203(C), pages 506-517.
    11. Magdalena Kachel & Artur Kraszkiewicz & Alaa Subr & Stanisław Parafiniuk & Artur Przywara & Milan Koszel & Grzegorz Zając, 2020. "Impact of the Type of Fertilization and the Addition of Glycerol on the Quality of Spring Rape Straw Pellets," Energies, MDPI, vol. 13(4), pages 1-11, February.
    12. Sever Akdağ, Ayşe & Atak, Onur & Atimtay, Aysel T. & Sanin, Faika Dilek, 2018. "Co-combustion of sewage sludge from different treatment processes and a lignite coal in a laboratory scale combustor," Energy, Elsevier, vol. 158(C), pages 417-426.
    13. Link, Siim & Yrjas, Patrik & Hupa, Leena, 2018. "Ash melting behaviour of wheat straw blends with wood and reed," Renewable Energy, Elsevier, vol. 124(C), pages 11-20.

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