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Investigation of cellulose supramolecular structure changes during conversion of waste paper in near-critical water on producing 5-hydroxymethyl furfural

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  • Wan, Jinquan
  • Lian, Jie
  • Wang, Yan
  • Ma, Yongwen

Abstract

Waste paper as a kind of biomass contains a great quantity of cellulose which is a renewable energy resource. However, complex cellulose supramolecular structure restricts the conversion of waste paper in near-critical water. This study aimed to investigate the change characteristics of cellulose supramolecular structure (hydrogen bond models and crystallinity) during hydrolysis and its effects on 5-HMF yield. Waste paper has been treated in near-critical water at 375 °C and 22.5 MPa for a reaction time (160–240 s) and correlation between 5-HMF yield and the supramolecular structure of cellulose residues has been built up. The 5-HMF yield was increased with the increase of intermolecular hydrogen bonds content in cellulose residues and was increased first and then decreased with the increase of crystallinity of cellulose residues. The rate of decrystallization was out of sync with that of depolymerization, which also influenced 5-HMF yield. Reaction time can be a macro method to adjust the supramolecular structure of cellulose during the conversion of waste paper to obtain more 5-HMF. It showed that 5-HMF yield reached maximum 9.41% ± 0.47% when the intermolecular hydrogen bonds content of cellulose in residue was 67.77% and the crystallinity of cellulose in residue was 57.14% at 200 s.

Suggested Citation

  • Wan, Jinquan & Lian, Jie & Wang, Yan & Ma, Yongwen, 2015. "Investigation of cellulose supramolecular structure changes during conversion of waste paper in near-critical water on producing 5-hydroxymethyl furfural," Renewable Energy, Elsevier, vol. 80(C), pages 132-139.
    • Handle: RePEc:eee:renene:v:80:y:2015:i:c:p:132-139
    DOI: 10.1016/j.renene.2015.01.071
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    References listed on IDEAS

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    1. Mizi Fan, 2012. "Fourier Transform Infrared Spectroscopy for Natural Fibres," Chapters, in: Salih Mohammed Salih (ed.), Fourier Transform - Materials Analysis, IntechOpen.
    2. Goyal, H.B. & Seal, Diptendu & Saxena, R.C., 2008. "Bio-fuels from thermochemical conversion of renewable resources: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 12(2), pages 504-517, February.
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    1. Wang, Shuai & Eberhardt, Thomas L. & Guo, Dayi & Feng, Junfeng & Pan, Hui, 2022. "Efficient conversion of glucose into 5-HMF catalyzed by lignin-derived mesoporous carbon solid acid in a biphasic system," Renewable Energy, Elsevier, vol. 190(C), pages 1-10.
    2. Modak, Arindam & Mankar, Akshay R. & Sonde, R.R. & Pant, Kamal K., 2023. "One-pot conversion of glucose to 5-hydroxymethylfurfural under aqueous conditions using acid/base bifunctional mesoporous silica catalyst," Renewable Energy, Elsevier, vol. 212(C), pages 97-110.
    3. Lin, Jianying & Liu, Qiyu & Guan, Mingzhao & Liang, Haotong & Chen, Panpan & Ma, Qiaozhi & Jiang, Enchen, 2023. "Autohydrolysis pretreatment of corn stalk for improved 5-hydroxymethylfurfural production in molten salt hydrate/acetone," Renewable Energy, Elsevier, vol. 217(C).

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