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Autohydrolysis pretreatment of corn stalk for improved 5-hydroxymethylfurfural production in molten salt hydrate/acetone

Author

Listed:
  • Lin, Jianying
  • Liu, Qiyu
  • Guan, Mingzhao
  • Liang, Haotong
  • Chen, Panpan
  • Ma, Qiaozhi
  • Jiang, Enchen

Abstract

Molten salt hydrate (MSH) is unique in cellulose dissolution and in one-pot conversion of crystalline cellulose into 5-hydroxymethylfurfural (5-HMF). However, low yield of 5-HMF was obtained using raw biomass substrate in MSHs. Herein, we investigated conversion of raw biomass towards HMF using MSHs. We showed that the release of acetic acid from hemicellulose degradation in MSH is a key to influence the yield of 5-HMF. Thus, an autohydrolysis pretreatment method was proposed to remove hemicellulose before conversion of cellulose into 5-HMF. After being pretreated at 180 °C for 40 min, hemicellulose was removed from biomass with 91.8% yield of cellulose remained in solid part. By eliminating the negative effect of acetic acid, 5-HMF yield was significantly improved from 40.9% to 64.6%, together with 9.3% yield of glucose for cellulose conversion in MSH/acetone at 180 °C for 20 min.

Suggested Citation

  • Lin, Jianying & Liu, Qiyu & Guan, Mingzhao & Liang, Haotong & Chen, Panpan & Ma, Qiaozhi & Jiang, Enchen, 2023. "Autohydrolysis pretreatment of corn stalk for improved 5-hydroxymethylfurfural production in molten salt hydrate/acetone," Renewable Energy, Elsevier, vol. 217(C).
    • Handle: RePEc:eee:renene:v:217:y:2023:i:c:s0960148123011369
    DOI: 10.1016/j.renene.2023.119221
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    References listed on IDEAS

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    1. Wan, Jinquan & Lian, Jie & Wang, Yan & Ma, Yongwen, 2015. "Investigation of cellulose supramolecular structure changes during conversion of waste paper in near-critical water on producing 5-hydroxymethyl furfural," Renewable Energy, Elsevier, vol. 80(C), pages 132-139.
    2. Bains, Rohit & Kumar, Ajay & Chauhan, Arvind Singh & Das, Pralay, 2022. "Dimethyl carbonate solvent assisted efficient conversion of lignocellulosic biomass to 5- hydroxymethylfurfural and furfural," Renewable Energy, Elsevier, vol. 197(C), pages 237-243.
    3. Sert, Murat & Arslanoğlu, Alparslan & Ballice, Levent, 2018. "Conversion of sunflower stalk based cellulose to the valuable products using choline chloride based deep eutectic solvents," Renewable Energy, Elsevier, vol. 118(C), pages 993-1000.
    4. Kim, Juyeon & Byun, Jaewon & Han, Jeehoon, 2022. "Process integration and economics of gamma-valerolactone using a cellulose-derived ethyl levulinate intermediate and ethanol solvent," Energy, Elsevier, vol. 239(PA).
    5. Lu, Qiaomin & Yan, Dong & Wu, Peiwen & Chen, Li & Yagoub, Abu ElGasim A. & Ji, Qinghua & Yu, Xiaojie & Zhou, Cunshan, 2022. "Ultrasound-NATDES/DMSO system for corn straw biomass conversion into platform compounds," Renewable Energy, Elsevier, vol. 190(C), pages 675-683.
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