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Preparation and characterization of Ni-M (M: Ru, Rh, Pd) nanoclusters as efficient catalysts for hydrogen evolution from ammonia borane methanolysis

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  • Tunç, Nihat
  • Rakap, Murat

Abstract

Here, first-time preparation, characterization, and catalytic use of hydroxyapatite-supported nickel-based Ni-M (NiRu@HAP, NiRh@HAP, NiPd@HAP) nanoclusters in hydrogen evolution from methanolysis of ammonia borane is reported. Ni-M nanoclusters have been in-situ formed by reduction of hydroxyapatite-supported corresponding metal ions during methanolysis reaction of ammonia borane. The hydroxyapatite-supported Ni-M nanoclusters are isolated as stable solid materials to be characterized by advanced analytical techniques of ICP-OES, TEM, XPS, and XRD. They are found to be isolable, highly redispersible and reusable nanocatalysts for hydrogen evolution from ammonia borane methanolysis under ambient conditions. Ni20Ru80@HAP, Ni38Rh62@HAP, and Ni20Pd80@HAP nanoclusters have TOF values of 58.9, 120.3, and 25.2 min−1, respectively, in the methanolysis of ammonia borane at 25 ± 0.1 °C. Their apparent activation energy (Ea) values for the same reaction are calculated to be 65.9, 66.8, and 58.1 kJ/mol, respectively, for Ni20Ru80@HAP, Ni38Rh62@HAP, and Ni20Pd80@HAP nanoclusters.

Suggested Citation

  • Tunç, Nihat & Rakap, Murat, 2020. "Preparation and characterization of Ni-M (M: Ru, Rh, Pd) nanoclusters as efficient catalysts for hydrogen evolution from ammonia borane methanolysis," Renewable Energy, Elsevier, vol. 155(C), pages 1222-1230.
    • Handle: RePEc:eee:renene:v:155:y:2020:i:c:p:1222-1230
    DOI: 10.1016/j.renene.2020.04.079
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    1. A. C. Dillon & K. M. Jones & T. A. Bekkedahl & C. H. Kiang & D. S. Bethune & M. J. Heben, 1997. "Storage of hydrogen in single-walled carbon nanotubes," Nature, Nature, vol. 386(6623), pages 377-379, March.
    2. Ping Chen & Zhitao Xiong & Jizhong Luo & Jianyi Lin & Kuang Lee Tan, 2002. "Interaction of hydrogen with metal nitrides and imides," Nature, Nature, vol. 420(6913), pages 302-304, November.
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    1. Komova, O.V. & Simagina, V.I. & Butenko, V.R. & Odegova, G.V. & Bulavchenko, O.A. & Nikolaeva, O.A. & Ozerova, A.M. & Lipatnikova, I.L. & Tayban, E.S. & Mukha, S.A. & Netskina, O.V., 2022. "Dehydrogenation of ammonia borane recrystallized by different techniques," Renewable Energy, Elsevier, vol. 184(C), pages 460-472.
    2. Feng, Yufa & Chen, Xiaodong & Wang, Huize & Li, Xiaolei & Huang, Hanzhao & Liu, Yu & Li, Hao, 2021. "Durable and high performing Ti supported Ni0.4Cu0.6Co2O4 nanoleaf-like array catalysts for hydrogen production," Renewable Energy, Elsevier, vol. 169(C), pages 660-669.
    3. Zhao, Liqing & Wei, Qinghe & Zhang, Lili & Zhao, Yafei & Zhang, Bing, 2021. "NiCo alloy decorated on porous N-doped carbon derived from ZnCo-ZIF as highly efficient and magnetically recyclable catalyst for hydrogen evolution from ammonia borane," Renewable Energy, Elsevier, vol. 173(C), pages 273-282.

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