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Structural analysis of bio-oils from sub-and supercritical water liquefaction of woody biomass

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  • Qian, Yejian
  • Zuo, Chengji
  • Tan, Jian
  • He, Jianhui

Abstract

Woody biomass was liquefied by water in an autoclave in the reaction temperature range of 280–420°C with sodium carbonate as the catalyst. The experimental results show that the yield of the main liquefaction product (heavy oil) was significantly influenced by the process conditions. The maximum yield of heavy oil was obtained at reaction temperature 380°C. The heavy oils obtained at different reaction temperature were analyzed by Fourier transform infrared spectroscopy (FTIR) and gas chromatography/mass spectrometry (GC/MS). The analytical results show the heavy oil is complex compound that contain hydrocarbon, aldehyde, ketone, hydroxybenzene and ester.

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  • Qian, Yejian & Zuo, Chengji & Tan, Jian & He, Jianhui, 2007. "Structural analysis of bio-oils from sub-and supercritical water liquefaction of woody biomass," Energy, Elsevier, vol. 32(3), pages 196-202.
    • Handle: RePEc:eee:energy:v:32:y:2007:i:3:p:196-202
    DOI: 10.1016/j.energy.2006.03.027
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    18. Wu, Haijun & Shakeel, Usama & Zhang, Quan & Zhang, Kai & Xu, Xia & Yuan, Yamei & Xu, Jian, 2022. "Catalytic degradation of poplar by Na2CO3 and Na2CO3/Fe under various hydrothermal liquefaction processes," Energy, Elsevier, vol. 259(C).
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    21. Yuan, X.Z. & Li, H. & Zeng, G.M. & Tong, J.Y. & Xie, W., 2007. "Sub- and supercritical liquefaction of rice straw in the presence of ethanol–water and 2-propanol–water mixture," Energy, Elsevier, vol. 32(11), pages 2081-2088.
    22. Leng, Lijian & Yuan, Xingzhong & Chen, Xiaohong & Huang, Huajun & Wang, Hou & Li, Hui & Zhu, Ren & Li, Shanxing & Zeng, Guangming, 2015. "Characterization of liquefaction bio-oil from sewage sludge and its solubilization in diesel microemulsion," Energy, Elsevier, vol. 82(C), pages 218-228.
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    25. Medrano, J.A. & Oliva, M. & Ruiz, J. & García, L. & Arauzo, J., 2011. "Hydrogen from aqueous fraction of biomass pyrolysis liquids by catalytic steam reforming in fluidized bed," Energy, Elsevier, vol. 36(4), pages 2215-2224.

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