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Microwave-assisted pyrolysis of furfural residue in a continuously operated auger reactor: Characterization and analyses of condensates and non-condensable gases

Author

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  • Kang, Qinhao
  • Mao, Xiao
  • Siyal, Asif Ali
  • Liu, Yang
  • Ran, Chunmei
  • Deng, Zeyu
  • Fu, Jie
  • Ao, Wenya
  • Song, Yongmeng
  • Dai, Jianjun

Abstract

Microwave-assisted pyrolysis of furfural residue (FR) in an auger reactor was conducted. The biochar yield decreased and non-condensable gas yield increased with increasing temperature. Condensate yield reached maximum (i.e. 21.49 wt%) at 550 °C. Kaolin, CaO and K2CO3 enhanced tar secondary reactions, reduced the yield and O/C ratio of bio-oil, improved GC-MS areas of phenolic compounds to 76.25%, 89.28% and 93.1%, respectively. All additives improved yields of H2 and CH4, while CaO reduced CO2. With increasing temperature, relative proportion (RP) of HCN/NH3 reached up to 13.67, while RP of H2S and chlorine in volatiles increased from 1.17%, 5.97% to 2.75%, 9.00%, respectively. Ammonia nitrogen in volatiles increased to 6.94% by K2CO3. Kaolin improved RP of HCN from 0.11% to 5.47%, while K2CO3 eliminated HCN. H2S increased with kaolin addition and decreased with CaO and K2CO3. Electricity consumption of MWAP varied from 0.5 to 3.78 (kWh/kg FR) depending on temperatures and additives.

Suggested Citation

  • Kang, Qinhao & Mao, Xiao & Siyal, Asif Ali & Liu, Yang & Ran, Chunmei & Deng, Zeyu & Fu, Jie & Ao, Wenya & Song, Yongmeng & Dai, Jianjun, 2019. "Microwave-assisted pyrolysis of furfural residue in a continuously operated auger reactor: Characterization and analyses of condensates and non-condensable gases," Energy, Elsevier, vol. 187(C).
    • Handle: RePEc:eee:energy:v:187:y:2019:i:c:s0360544219317980
    DOI: 10.1016/j.energy.2019.116103
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    1. Luo, Juan & Sun, Shichang & Chen, Xing & Lin, Junhao & Ma, Rui & Zhang, Rui & Fang, Lin, 2021. "In-depth exploration of the energy utilization and pyrolysis mechanism of advanced continuous microwave pyrolysis," Applied Energy, Elsevier, vol. 292(C).
    2. Scarlett Allende & Graham Brodie & Mohan V. Jacob, 2023. "Energy Recovery from Pumpkin Peel Using Microwave-Assisted Pyrolysis," Energies, MDPI, vol. 16(18), pages 1-11, September.
    3. Yong Sun & Zhi Wang & Yuyingnan Liu & Xianghui Meng & Jingbo Qu & Changyu Liu & Bin Qu, 2019. "A Review on the Transformation of Furfural Residue for Value-Added Products," Energies, MDPI, vol. 13(1), pages 1-19, December.
    4. Mohsin Raza & Abrar Inayat & Ashfaq Ahmed & Farrukh Jamil & Chaouki Ghenai & Salman R. Naqvi & Abdallah Shanableh & Muhammad Ayoub & Ammara Waris & Young-Kwon Park, 2021. "Progress of the Pyrolyzer Reactors and Advanced Technologies for Biomass Pyrolysis Processing," Sustainability, MDPI, vol. 13(19), pages 1-42, October.

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