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Lattice Expansion and Crystallite Size Analyses of NiO-BaCe 0. 54 Zr 0. 36 Y 0. 1 O 3-δ Anode Composite for Proton Ceramic Fuel Cells Application

Author

Listed:
  • Nurul Waheeda Mazlan

    (Proton Conducting Fuel Cell Group, Universiti Teknologi MARA, Shah Alam 40450, Selangor, Malaysia)

  • Munirah Shafiqah Murat

    (Faculty of Applied Sciences, Universiti Teknologi MARA, Arau 02600, Perlis, Malaysia)

  • Chung-Jen Tseng

    (Center for Energy Research, National Central University, No. 300, Zhongda Rd., Zhongli District, Taoyuan City 320317, Taiwan)

  • Oskar Hasdinor Hassan

    (Institute of Science, Universiti Teknologi MARA, Shah Alam 40450, Selangor, Malaysia)

  • Nafisah Osman

    (Proton Conducting Fuel Cell Group, Universiti Teknologi MARA, Shah Alam 40450, Selangor, Malaysia
    Faculty of Applied Sciences, Universiti Teknologi MARA, Arau 02600, Perlis, Malaysia)

Abstract

This study reports on the structure analyses of NiO-BCZY (BCZY = BaCe 0. 54 Zr 0. 36 Y 0. 1 O 3-δ ) anode composite materials with the ratio of 50:50 for proton ceramic fuel cells (PCFCs) application. A product of sintered NiO-BCZY was developed to understand the structural properties of the anode materials. The objectives of this work were (a) to investigate the lattice expansion of the anode by using a high-temperature XRD (HT-XRD) from 400–700 °C; and (b) to calculate the crystallite size of the sample by using Scherrer’s and Williamson Hall’s methods. The results obtained from the HT-XRD revealed that the diffraction peaks of NiO and BCZY are matched with the cubic phase perovskite structure. For example at T = 400 °C, the lattice parameter of NiO is a = 4.2004 Å and BCZY is a = 4.3331 Å. The observation also showed that the lattice expansion increased with the temperature. Furthermore, analyses of the Scherrer and Williamson Hall methods, respectively, showed that the crystallite size is strongly correlated with the lattice expansion, which proved that the crystallite size increased as the operating temperature increased. The increment of crystallite size over the operating temperature contributed to the increment of conductivity values of the single cell.

Suggested Citation

  • Nurul Waheeda Mazlan & Munirah Shafiqah Murat & Chung-Jen Tseng & Oskar Hasdinor Hassan & Nafisah Osman, 2022. "Lattice Expansion and Crystallite Size Analyses of NiO-BaCe 0. 54 Zr 0. 36 Y 0. 1 O 3-δ Anode Composite for Proton Ceramic Fuel Cells Application," Energies, MDPI, vol. 15(22), pages 1-10, November.
    • Handle: RePEc:gam:jeners:v:15:y:2022:i:22:p:8520-:d:972675
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    References listed on IDEAS

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    1. Hong Liu & Zoheb Akhtar & Peiwen Li & Kai Wang, 2014. "Mathematical Modeling Analysis and Optimization of Key Design Parameters of Proton-Conductive Solid Oxide Fuel Cells," Energies, MDPI, vol. 7(1), pages 1-18, January.
    2. Raluca-Andreea Felseghi & Elena Carcadea & Maria Simona Raboaca & Cătălin Nicolae TRUFIN & Constantin Filote, 2019. "Hydrogen Fuel Cell Technology for the Sustainable Future of Stationary Applications," Energies, MDPI, vol. 12(23), pages 1-28, December.
    3. Ahmad Fuzamy Mohd Abd Fatah & Ahmad Zaki Rosli & Ahmad Azmin Mohamad & Andanastuti Muchtar & Muhammed Ali S.A. & Noorashrina A. Hamid, 2022. "Electrochemical Evaluation of Nickel Oxide Addition toward Lanthanum Strontium Cobalt Ferrite Cathode for Intermediate Temperature Solid Oxide Fuel Cell (IT-SOFCS)," Energies, MDPI, vol. 15(14), pages 1-15, July.
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