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Optimization of biodiesel production process from Jatropha oil using supported heteropolyacid catalyst and assisted by ultrasonic energy

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  • Badday, Ali Sabri
  • Abdullah, Ahmad Zuhairi
  • Lee, Keat-Teong

Abstract

Application of ultrasound-assisted biodiesel production process from Jatropha oil catalyzed by activated carbon-supported tungstophosphoric acid catalyst was studied. Influences of ultrasonic energy on different process variables were elucidated. Reaction variables i.e. reaction time (10–50 min), reactants' molar ratio (5:1–25:1), ultrasonic amplitude (30–90% of the maximum sonifier power) and catalyst amount (2.5–4.5 w/w oil) were studied. A mathematical representation for biodiesel yield was successfully generated. A yield of 91% was achieved in just 40 min at a moderate ultrasonic amplitude (∼60%), high molar ratio (25:1) and low reaction temperature (65 °C). Interactions between the variables were also validated statistically. Leaching study revealed that the reaction was predominately heterogeneous in nature.

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  • Badday, Ali Sabri & Abdullah, Ahmad Zuhairi & Lee, Keat-Teong, 2013. "Optimization of biodiesel production process from Jatropha oil using supported heteropolyacid catalyst and assisted by ultrasonic energy," Renewable Energy, Elsevier, vol. 50(C), pages 427-432.
    • Handle: RePEc:eee:renene:v:50:y:2013:i:c:p:427-432
    DOI: 10.1016/j.renene.2012.07.013
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    5. Nayak, Milap G. & Vyas, Amish P., 2019. "Optimization of microwave-assisted biodiesel production from Papaya oil using response surface methodology," Renewable Energy, Elsevier, vol. 138(C), pages 18-28.
    6. Vávra, Aleš & Hájek, Martin & Skopal, Frantisek, 2017. "The removal of free fatty acids from methyl ester," Renewable Energy, Elsevier, vol. 103(C), pages 695-700.
    7. Avhad, M.R. & Marchetti, J.M., 2015. "A review on recent advancement in catalytic materials for biodiesel production," Renewable and Sustainable Energy Reviews, Elsevier, vol. 50(C), pages 696-718.
    8. Singh, Bhaskar & Guldhe, Abhishek & Rawat, Ismail & Bux, Faizal, 2014. "Towards a sustainable approach for development of biodiesel from plant and microalgae," Renewable and Sustainable Energy Reviews, Elsevier, vol. 29(C), pages 216-245.
    9. Badday, Ali Sabri & Abdullah, Ahmad Zuhairi & Lee, Keat-Teong, 2013. "Ultrasound-assisted transesterification of crude Jatropha oil using cesium doped heteropolyacid catalyst: Interactions between process variables," Energy, Elsevier, vol. 60(C), pages 283-291.

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