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Determination of the specific heat of biomass materials and the combustion energy of coke by DSC analysis

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  • Collazo, Joaquín
  • Pazó, José Antonio
  • Granada, Enrique
  • Saavedra, Ángeles
  • Eguía, Pablo

Abstract

The accurate determination of the thermal properties of biomass materials is particularly important when studying biomass combustion processes. This paper reports a method for the determination of the maximum sampling error and the confidence intervals of thermal properties obtained from TG–DSC analysis. Special care must be taken with the sampling procedure to achieve an acceptable degree of error and low statistical uncertainty. The obtained levels of uncertainty and error demonstrate that the properties evaluated by the analysis were representative of the fuels. A study of the trends and time correlations was performed to ensure that the observed correlations arise from completely random causes. The obtained results are particularly interesting for biomass energy applications.

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  • Collazo, Joaquín & Pazó, José Antonio & Granada, Enrique & Saavedra, Ángeles & Eguía, Pablo, 2012. "Determination of the specific heat of biomass materials and the combustion energy of coke by DSC analysis," Energy, Elsevier, vol. 45(1), pages 746-752.
    • Handle: RePEc:eee:energy:v:45:y:2012:i:1:p:746-752
    DOI: 10.1016/j.energy.2012.07.018
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    2. María E. Arce & Ángeles Saavedra & José L. Míguez & Enrique Granada & Antón Cacabelos, 2013. "Biomass Fuel and Combustion Conditions Selection in a Fixed Bed Combustor," Energies, MDPI, vol. 6(11), pages 1-17, November.
    3. López-González, D. & Avalos-Ramirez, A. & Giroir-Fendler, A. & Godbout, S. & Fernandez-Lopez, M. & Sanchez-Silva, L. & Valverde, J.L., 2015. "Combustion kinetic study of woody and herbaceous crops by thermal analysis coupled to mass spectrometry," Energy, Elsevier, vol. 90(P2), pages 1626-1635.
    4. Wander, Paulo R. & Bianchi, Flávio M. & Caetano, Nattan R. & Klunk, Marcos A. & Indrusiak, Maria Luiza S., 2020. "Cofiring low-rank coal and biomass in a bubbling fluidized bed with varying excess air ratio and fluidization velocity," Energy, Elsevier, vol. 203(C).
    5. Fonseca, Frederico G. & Soares Dias, Ana P., 2021. "Almond shells: Catalytic fixed-bed pyrolysis and volatilization kinetics," Renewable Energy, Elsevier, vol. 180(C), pages 1380-1390.

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