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Upgrading of pinyon-juniper catalytic pyrolysis oil via hydrodeoxygenation

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  • Jahromi, Hossein
  • Agblevor, Foster A.

Abstract

In this study we discuss hydrodeoxygenation (HDO) of pinyon juniper (PJ) catalytic pyrolysis oil over Ni/SiO2Al2O3 catalyst in a batch reactor to improve the physicochemical properties of the oil. The influence of temperature (350–500 °C), reaction time (15–90 min), and initial hydrogen pressure (3.5–10 MPa), on hydrodeoxygenation of PJ pyrolysis oil was investigated. After hydrogenation was completed, gas, coke, and a liquid product of two immiscible phases (aqueous and organic), were obtained. Maximum HDO of bio-oil was achieved at 450° C while the initial hydrogen pressure was 7 MPa and the reaction time was 30 min. Under these conditions, the H/C and O/C atomic ratios changed from 1.29 to 0.29 respectively for bio-oil to 2.36 and 0 for HDO oil respectively. The higher heating value increased from 27.64 MJ/kg of bio-oil to 45.58 MJ/kg of upgraded oil. The water content of organic liquid product was less than 0.05 wt% while it was 1.63 wt% in the feed. The viscosity of upgraded oil was 1.26 cP compared to119 cP for the crude bio-oil.

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  • Jahromi, Hossein & Agblevor, Foster A., 2017. "Upgrading of pinyon-juniper catalytic pyrolysis oil via hydrodeoxygenation," Energy, Elsevier, vol. 141(C), pages 2186-2195.
    • Handle: RePEc:eee:energy:v:141:y:2017:i:c:p:2186-2195
    DOI: 10.1016/j.energy.2017.11.149
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    2. Li, Zhixia & Huang, Zhentao & Ding, Shilei & Li, Fuwei & Wang, Zhaohe & Lin, Hongfei & Chen, Congjin, 2018. "Catalytic conversion of waste cooking oil to fuel oil: Catalyst design and effect of solvent," Energy, Elsevier, vol. 157(C), pages 270-277.
    3. Ochoa, Aitor & Vicente, Héctor & Sierra, Irene & Arandes, José M. & Castaño, Pedro, 2020. "Implications of feeding or cofeeding bio-oil in the fluid catalytic cracker (FCC) in terms of regeneration kinetics and energy balance," Energy, Elsevier, vol. 209(C).
    4. Kumar, R. & Strezov, V., 2021. "Thermochemical production of bio-oil: A review of downstream processing technologies for bio-oil upgrading, production of hydrogen and high value-added products," Renewable and Sustainable Energy Reviews, Elsevier, vol. 135(C).

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