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Preparation of methyl levulinate from fractionation of direct liquefied bamboo biomass

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  • Feng, Junfeng
  • Jiang, Jianchun
  • Xu, Junming
  • Yang, Zhongzhi
  • Wang, Kui
  • Guan, Qian
  • Chen, Shuigen

Abstract

One-step preparation of methyl levulinate from biomass was investigated. The process used was direct liquefaction under pressure in methanol using a 1L autoclave. Bamboo, a lignocellulosic biomass, was liquefied using sulfuric acid in subcritical methanol. When sulfuric acid was used as the catalyst, a 30.75wt% methyl levulinate yield could be obtained from bamboo at 200°C after a reaction time of 120min when the catalyst loading was 2.5wt% per 60g bamboo. In addition, microcrystalline cellulose, corn starch, methyl glucoside and glucose were selected as model compounds for the liquefaction reaction so that the biomass to methyl levulinate reaction pathway could be investigated. The results suggested that lignocellulosic biomass is a renewable material that can be used to produce a high value-added fuel additive (methyl levulinate) by the direct liquefaction under pressure reaction process.

Suggested Citation

  • Feng, Junfeng & Jiang, Jianchun & Xu, Junming & Yang, Zhongzhi & Wang, Kui & Guan, Qian & Chen, Shuigen, 2015. "Preparation of methyl levulinate from fractionation of direct liquefied bamboo biomass," Applied Energy, Elsevier, vol. 154(C), pages 520-527.
    • Handle: RePEc:eee:appene:v:154:y:2015:i:c:p:520-527
    DOI: 10.1016/j.apenergy.2015.04.115
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    References listed on IDEAS

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    1. Zhao, Weijie & Li, Yingwen & Song, Changhua & Liu, Sijie & Li, Xuehui & Long, Jinxing, 2017. "Intensified levulinic acid/ester production from cassava by one-pot cascade prehydrolysis and delignification," Applied Energy, Elsevier, vol. 204(C), pages 1094-1100.
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    3. Samanta, Ritika & Chakraborty, Rajat, 2023. "Methyl levulinate synthesis from rice husk employing e-waste derived silica supported nano CuO–CdSO4 photocatalyst: Assessment of production environmental impacts, engine performance and emissions," Renewable Energy, Elsevier, vol. 210(C), pages 842-858.

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