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Cyclic Subcritical Water Injection into Bazhenov Oil Shale: Geochemical and Petrophysical Properties Evolution Due to Hydrothermal Exposure

Author

Listed:
  • Aman Turakhanov

    (Skolkovo Institute of Science and Technology, 121205 Moscow, Russia)

  • Albina Tsyshkova

    (Skolkovo Institute of Science and Technology, 121205 Moscow, Russia)

  • Elena Mukhina

    (Skolkovo Institute of Science and Technology, 121205 Moscow, Russia)

  • Evgeny Popov

    (Skolkovo Institute of Science and Technology, 121205 Moscow, Russia)

  • Darya Kalacheva

    (Gazpromneft STC (Science & Technology Centre), 190000 Saint Petersburg, Russia)

  • Ekaterina Dvoretskaya

    (Gazpromneft STC (Science & Technology Centre), 190000 Saint Petersburg, Russia)

  • Anton Kasyanenko

    (Bazhen TC (Technology Centre), 190000 Saint Petersburg, Russia)

  • Konstantin Prochukhan

    (Bazhen TC (Technology Centre), 190000 Saint Petersburg, Russia)

  • Alexey Cheremisin

    (Skolkovo Institute of Science and Technology, 121205 Moscow, Russia)

Abstract

In situ shale or kerogen oil production is a promising approach to developing vast oil shale resources and increasing world energy demand. In this study, cyclic subcritical water injection in oil shale was investigated in laboratory conditions as a method for in situ oil shale retorting. Fifteen non-extracted oil shale samples from Bazhenov Formation in Russia (98 °C and 23.5 MPa reservoir conditions) were hydrothermally treated at 350 °C and in a 25 MPa semi-open system during 50 h in the cyclic regime. The influence of the artificial maturation on geochemical parameters, elastic and microstructural properties was studied. Rock-Eval pyrolysis of non-extracted and extracted oil shale samples before and after hydrothermal exposure and SARA analysis were employed to analyze bitumen and kerogen transformation to mobile hydrocarbons and immobile char. X-ray computed microtomography (XMT) was performed to characterize the microstructural properties of pore space. The results demonstrated significant porosity, specific pore surface area increase, and the appearance of microfractures in organic-rich layers. Acoustic measurements were carried out to estimate the alteration of elastic properties due to hydrothermal treatment. Both Young’s modulus and Poisson’s ratio decreased due to kerogen transformation to heavy oil and bitumen, which remain trapped before further oil and gas generation, and expulsion occurs. Ultimately, a developed kinetic model was applied to match kerogen and bitumen transformation with liquid and gas hydrocarbons production. The nonlinear least-squares optimization problem was solved during the integration of the system of differential equations to match produced hydrocarbons with pyrolysis derived kerogen and bitumen decomposition.

Suggested Citation

  • Aman Turakhanov & Albina Tsyshkova & Elena Mukhina & Evgeny Popov & Darya Kalacheva & Ekaterina Dvoretskaya & Anton Kasyanenko & Konstantin Prochukhan & Alexey Cheremisin, 2021. "Cyclic Subcritical Water Injection into Bazhenov Oil Shale: Geochemical and Petrophysical Properties Evolution Due to Hydrothermal Exposure," Energies, MDPI, vol. 14(15), pages 1-16, July.
    • Handle: RePEc:gam:jeners:v:14:y:2021:i:15:p:4570-:d:603376
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    References listed on IDEAS

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    1. Pan-Sang Kang & Jong-Se Lim & Chun Huh, 2016. "Screening Criteria and Considerations of Offshore Enhanced Oil Recovery," Energies, MDPI, vol. 9(1), pages 1-18, January.
    2. Saif, Tarik & Lin, Qingyang & Gao, Ying & Al-Khulaifi, Yousef & Marone, Federica & Hollis, David & Blunt, Martin J. & Bijeljic, Branko, 2019. "4D in situ synchrotron X-ray tomographic microscopy and laser-based heating study of oil shale pyrolysis," Applied Energy, Elsevier, vol. 235(C), pages 1468-1475.
    3. Thiruvenkadam, Selvakumar & Izhar, Shamsul & Yoshida, Hiroyuki & Danquah, Michael K. & Harun, Razif, 2015. "Process application of Subcritical Water Extraction (SWE) for algal bio-products and biofuels production," Applied Energy, Elsevier, vol. 154(C), pages 815-828.
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    Cited by:

    1. Desmond Batsa Dorhjie & Elena Mukhina & Anton Kasyanenko & Alexey Cheremisin, 2023. "Tight and Shale Oil Exploration: A Review of the Global Experience and a Case of West Siberia," Energies, MDPI, vol. 16(18), pages 1-28, September.
    2. Reza Rezaee, 2022. "Editorial on Special Issues of Development of Unconventional Reservoirs," Energies, MDPI, vol. 15(7), pages 1-9, April.
    3. Golam Muktadir & Moh’d Amro & Nicolai Kummer & Carsten Freese & Khizar Abid, 2021. "Application of X-ray Diffraction (XRD) and Rock–Eval Analysis for the Evaluation of Middle Eastern Petroleum Source Rock," Energies, MDPI, vol. 14(20), pages 1-16, October.

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