IDEAS home Printed from https://ideas.repec.org/a/gam/jeners/v11y2018i10p2505-d171163.html
   My bibliography  Save this article

Experimental Method and Setup for Laboratory Fluidized Bed Reactor Testing

Author

Listed:
  • Henrik Leion

    (Energy and Materials, Chemistry and Chemical Engineering, Chalmers University of Technology, 412 96 Gothenburg, Sweden)

  • Volkmar Frick

    (Energy and Materials, Chemistry and Chemical Engineering, Chalmers University of Technology, 412 96 Gothenburg, Sweden)

  • Fredrik Hildor

    (Energy and Materials, Chemistry and Chemical Engineering, Chalmers University of Technology, 412 96 Gothenburg, Sweden)

Abstract

A small laboratory fluidized bed reactor is used to test the chemical reactivity of solid particles fluidized with a gas. The novelty of the system is that it can be used for testing any solid particles, and, in this work, oxygen carriers with Mn/Si oxide supported on TiO 2 are used to present the possibilities and layout of the laboratory system. The system is equipped with automatic valves that make it possible to rapidly change the gas conditions in the reactor. The setup facilitates solid particle testing using a sample of a few grams with gas-solid contact conditions relevant for a full-scale fluidized bed. With this small system, it is possible to mimic a section or a part of a larger system. It is also possible to test extreme conditions that can occur in a bigger unit. The system is designed for determining chemical reactivity in combustion, gasification, and reforming, but it can be used for investigating any type of gas-solid reaction in fluidized bed conditions. The setup presented here is one of the smallest possible devices that can be realized while maintaining fluidized bed conditions.

Suggested Citation

  • Henrik Leion & Volkmar Frick & Fredrik Hildor, 2018. "Experimental Method and Setup for Laboratory Fluidized Bed Reactor Testing," Energies, MDPI, vol. 11(10), pages 1-17, September.
  • Handle: RePEc:gam:jeners:v:11:y:2018:i:10:p:2505-:d:171163
    as

    Download full text from publisher

    File URL: https://www.mdpi.com/1996-1073/11/10/2505/pdf
    Download Restriction: no

    File URL: https://www.mdpi.com/1996-1073/11/10/2505/
    Download Restriction: no
    ---><---

    References listed on IDEAS

    as
    1. Rydén, Magnus & Leion, Henrik & Mattisson, Tobias & Lyngfelt, Anders, 2014. "Combined oxides as oxygen-carrier material for chemical-looping with oxygen uncoupling," Applied Energy, Elsevier, vol. 113(C), pages 1924-1932.
    2. Frick, Volkmar & Rydén, Magnus & Leion, Henrik & Mattisson, Tobias & Lyngfelt, Anders, 2015. "Screening of supported and unsupported Mn–Si oxygen carriers for CLOU (chemical-looping with oxygen uncoupling)," Energy, Elsevier, vol. 93(P1), pages 544-554.
    Full references (including those not matched with items on IDEAS)

    Citations

    Citations are extracted by the CitEc Project, subscribe to its RSS feed for this item.
    as


    Cited by:

    1. Fredrik Hildor & Henrik Leion & Tobias Mattisson, 2022. "Steel Converter Slag as an Oxygen Carrier—Interaction with Sulfur Dioxide," Energies, MDPI, vol. 15(16), pages 1-29, August.

    Most related items

    These are the items that most often cite the same works as this one and are cited by the same works as this one.
    1. Schmitz, Matthias & Linderholm, Carl Johan, 2016. "Performance of calcium manganate as oxygen carrier in chemical looping combustion of biochar in a 10kW pilot," Applied Energy, Elsevier, vol. 169(C), pages 729-737.
    2. Kang, Dohyung & Lim, Hyun Suk & Lee, Minbeom & Lee, Jae W., 2018. "Syngas production on a Ni-enhanced Fe2O3/Al2O3 oxygen carrier via chemical looping partial oxidation with dry reforming of methane," Applied Energy, Elsevier, vol. 211(C), pages 174-186.
    3. Zhao, Haibo & Guo, Lei & Zou, Xixian, 2015. "Chemical-looping auto-thermal reforming of biomass using Cu-based oxygen carrier," Applied Energy, Elsevier, vol. 157(C), pages 408-415.
    4. Li, Fang-zhou & Kang, Jing-xian & Song, Yun-cai & Feng, Jie & Li, Wen-ying, 2020. "Thermodynamic feasibility for molybdenum-based gaseous oxides assisted looping coal gasification and its derived power plant," Energy, Elsevier, vol. 194(C).
    5. Galinsky, Nathan & Mishra, Amit & Zhang, Jia & Li, Fanxing, 2015. "Ca1−xAxMnO3 (A=Sr and Ba) perovskite based oxygen carriers for chemical looping with oxygen uncoupling (CLOU)," Applied Energy, Elsevier, vol. 157(C), pages 358-367.
    6. Ping Wang & Nicholas Means & Dushyant Shekhawat & David Berry & Mehrdad Massoudi, 2015. "Chemical-Looping Combustion and Gasification of Coals and Oxygen Carrier Development: A Brief Review," Energies, MDPI, vol. 8(10), pages 1-31, September.
    7. Galinsky, Nathan & Sendi, Marwan & Bowers, Lindsay & Li, Fanxing, 2016. "CaMn1−xBxO3−δ (B=Al, V, Fe, Co, and Ni) perovskite based oxygen carriers for chemical looping with oxygen uncoupling (CLOU)," Applied Energy, Elsevier, vol. 174(C), pages 80-87.
    8. Abad, A. & Pérez-Vega, R. & de Diego, L.F. & Gayán, P. & Izquierdo, M.T. & García-Labiano, F. & Adánez, J., 2019. "Thermochemical assessment of chemical looping assisted by oxygen uncoupling with a MnFe-based oxygen carrier," Applied Energy, Elsevier, vol. 251(C), pages 1-1.
    9. Hu, Wenting & Donat, Felix & Scott, S.A. & Dennis, J.S., 2016. "Kinetics of oxygen uncoupling of a copper based oxygen carrier," Applied Energy, Elsevier, vol. 161(C), pages 92-100.
    10. Huang, Jijiang & Liu, Wen & Hu, Wenting & Metcalfe, Ian & Yang, Yanhui & Liu, Bin, 2019. "Phase interactions in Ni-Cu-Al2O3 mixed oxide oxygen carriers for chemical looping applications," Applied Energy, Elsevier, vol. 236(C), pages 635-647.
    11. Xu, Lei & Sun, Hongming & Li, Zhenshan & Cai, Ningsheng, 2016. "Experimental study of copper modified manganese ores as oxygen carriers in a dual fluidized bed reactor," Applied Energy, Elsevier, vol. 162(C), pages 940-947.
    12. Di, Zichen & Yilmaz, Duygu & Biswas, Arijit & Cheng, Fangqin & Leion, Henrik, 2022. "Spinel ferrite-contained industrial materials as oxygen carriers in chemical looping combustion," Applied Energy, Elsevier, vol. 307(C).
    13. Zhao, Kun & Li, Luwei & Zheng, Anqing & Huang, Zhen & He, Fang & Shen, Yang & Wei, Guoqiang & Li, Haibin & Zhao, Zengli, 2017. "Synergistic improvements in stability and performance of the double perovskite-type oxides La2−xSrxFeCoO6 for chemical looping steam methane reforming," Applied Energy, Elsevier, vol. 197(C), pages 393-404.
    14. Tang, Mingchen & Xu, Long & Fan, Maohong, 2015. "Progress in oxygen carrier development of methane-based chemical-looping reforming: A review," Applied Energy, Elsevier, vol. 151(C), pages 143-156.
    15. Dizaji, Hossein Beidaghy & Hosseini, Hannaneh, 2018. "A review of material screening in pure and mixed-metal oxide thermochemical energy storage (TCES) systems for concentrated solar power (CSP) applications," Renewable and Sustainable Energy Reviews, Elsevier, vol. 98(C), pages 9-26.
    16. Albrecht, Kevin J. & Jackson, Gregory S. & Braun, Robert J., 2016. "Thermodynamically consistent modeling of redox-stable perovskite oxides for thermochemical energy conversion and storage," Applied Energy, Elsevier, vol. 165(C), pages 285-296.
    17. Zhao, Kun & He, Fang & Huang, Zhen & Wei, Guoqiang & Zheng, Anqing & Li, Haibin & Zhao, Zengli, 2016. "Perovskite-type oxides LaFe1−xCoxO3 for chemical looping steam methane reforming to syngas and hydrogen co-production," Applied Energy, Elsevier, vol. 168(C), pages 193-203.
    18. Pérez-Vega, R. & Abad, A. & Izquierdo, M.T. & Gayán, P. & de Diego, L.F. & Adánez, J., 2019. "Evaluation of Mn-Fe mixed oxide doped with TiO2 for the combustion with CO2 capture by Chemical Looping assisted by Oxygen Uncoupling," Applied Energy, Elsevier, vol. 237(C), pages 822-835.
    19. Siriwardane, Ranjani & Riley, Jarrett & Benincosa, William & Bayham, Samuel & Bobek, Michael & Straub, Douglas & Weber, Justin, 2021. "Development of CuFeMnAlO4+δ oxygen carrier with high attrition resistance and 50-kWth methane/air chemical looping combustion tests," Applied Energy, Elsevier, vol. 286(C).
    20. Tescari, S. & Singh, A. & Agrafiotis, C. & de Oliveira, L. & Breuer, S. & Schlögl-Knothe, B. & Roeb, M. & Sattler, C., 2017. "Experimental evaluation of a pilot-scale thermochemical storage system for a concentrated solar power plant," Applied Energy, Elsevier, vol. 189(C), pages 66-75.

    Corrections

    All material on this site has been provided by the respective publishers and authors. You can help correct errors and omissions. When requesting a correction, please mention this item's handle: RePEc:gam:jeners:v:11:y:2018:i:10:p:2505-:d:171163. See general information about how to correct material in RePEc.

    If you have authored this item and are not yet registered with RePEc, we encourage you to do it here. This allows to link your profile to this item. It also allows you to accept potential citations to this item that we are uncertain about.

    If CitEc recognized a bibliographic reference but did not link an item in RePEc to it, you can help with this form .

    If you know of missing items citing this one, you can help us creating those links by adding the relevant references in the same way as above, for each refering item. If you are a registered author of this item, you may also want to check the "citations" tab in your RePEc Author Service profile, as there may be some citations waiting for confirmation.

    For technical questions regarding this item, or to correct its authors, title, abstract, bibliographic or download information, contact: MDPI Indexing Manager (email available below). General contact details of provider: https://www.mdpi.com .

    Please note that corrections may take a couple of weeks to filter through the various RePEc services.

    IDEAS is a RePEc service. RePEc uses bibliographic data supplied by the respective publishers.