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Optimization of various pretreatments condition of kenaf core (Hibiscus cannabinus) fibre for sugar production: Effect of chemical compositions of pretreated fibre on enzymatic hydrolysability

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  • Tye, Ying Ying
  • Lee, Keat Teong
  • Wan Abdullah, Wan Nadiah
  • Leh, Cheu Peng

Abstract

In this work, the effects of various pretreatments’ parameters on kenaf core fibre were analyzed statistically and optimized using Response Surface Methodology based on the total glucose yield. The chemical compositions of the pretreated fibres were examined to discuss the effect of pretreatment on the fibre hydrolysability comprehensively. The results showed that estimation model for each pretreatment of kenaf core fibre were polynomial equations. The optimum conditions for water, acid and alkali pretreatments were 170 °C for 45 min, 120 °C for 90 min in 2.0% H2SO4 solution and 140 °C for 60 min in 3.0% NaOH solution, respectively. Among the three pretreatments, water pretreatment achieved the highest total glucose yield (25.5%), followed by acid (20.0%) and alkali (18.2%) pretreatments. Based on chemical compositions analysis, both water and acid pretreatments were capable of eliminating almost 100% of hemicellulose with negligible removal of lignin while the alkali pretreatment removed both the lignin and hemicellulose more than 60%. This result revealed that the removal of hemicellulose showed greater influential in enhancing the enzymatic accessibility and hence, hydrolysability of kenaf core fibre.

Suggested Citation

  • Tye, Ying Ying & Lee, Keat Teong & Wan Abdullah, Wan Nadiah & Leh, Cheu Peng, 2016. "Optimization of various pretreatments condition of kenaf core (Hibiscus cannabinus) fibre for sugar production: Effect of chemical compositions of pretreated fibre on enzymatic hydrolysability," Renewable Energy, Elsevier, vol. 99(C), pages 205-215.
    • Handle: RePEc:eee:renene:v:99:y:2016:i:c:p:205-215
    DOI: 10.1016/j.renene.2016.06.040
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    References listed on IDEAS

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    1. Ruiz, Héctor A. & Rodríguez-Jasso, Rosa M. & Fernandes, Bruno D. & Vicente, António A. & Teixeira, José A., 2013. "Hydrothermal processing, as an alternative for upgrading agriculture residues and marine biomass according to the biorefinery concept: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 21(C), pages 35-51.
    2. Jack P. C. Kleijnen, 2015. "Response Surface Methodology," International Series in Operations Research & Management Science, in: Michael C Fu (ed.), Handbook of Simulation Optimization, edition 127, chapter 0, pages 81-104, Springer.
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    1. Tye, Ying Ying & Leh, Cheu Peng & Wan Abdullah, Wan Nadiah, 2017. "Total glucose yield as the single response in optimizing pretreatments for Elaeis guineensis fibre enzymatic hydrolysis and its relationship with chemical composition of fibre," Renewable Energy, Elsevier, vol. 114(PB), pages 383-393.
    2. Duangporn Premjet & Suwanan Wongleang & Siripong Premjet, 2022. "Enhancing Glucose Recovery from Hibiscus cannabinus L. through Phosphoric Acid Pretreatment," Energies, MDPI, vol. 15(20), pages 1-15, October.

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