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1-(Carboxymethyl)pyridinium chloride as an acidic ionic liquid for rice straw effective pretreatment

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  • Abdolmaleki, Amir
  • Nabavizadeh, Sayed Sajad
  • Badbedast, Mehran

Abstract

Herein, a suitable pretreatment based on an acidic ionic liquid was employed for superior enzymatic hydrolysis of rice straw, which is regarded as an inexpensive, easily accessible, and renewable agricultural waste. Using 1-(carboxymethyl)pyridinium chloride as an acidic ionic liquid, containing, both acetate and chloride groups, a superior penetration between cellulose chains and a proper dissolution can be easily achieved. Different analyzes, including FT-IR, XRD, and SEM, were conducted, indicating restructuring and increased free volume between cellulose chains in rice straw. Following the proper pretreatment with the ionic liquid, the next step in the fermentation and enzymatic hydrolysis process was well conducted, and promising results were attained for biofuel productions. The effects of water as a co-solvent, pretreatment time (2, 3, 5 h), temperature (25, 90, 120 °C), and solid loading (5, 6, 15% w/w) were investigated for maximum ethanol production. The best results were obtained in 35% water, at room temperature, and 6% (w/w) solid loading for 3 h. The hydrolysis yield in ethanol production was improved to 62.2% of the theoretical maximum.

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  • Abdolmaleki, Amir & Nabavizadeh, Sayed Sajad & Badbedast, Mehran, 2021. "1-(Carboxymethyl)pyridinium chloride as an acidic ionic liquid for rice straw effective pretreatment," Renewable Energy, Elsevier, vol. 177(C), pages 544-553.
    • Handle: RePEc:eee:renene:v:177:y:2021:i:c:p:544-553
    DOI: 10.1016/j.renene.2021.05.158
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    References listed on IDEAS

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    1. Devendra, Leena P. & Pandey, Ashok, 2016. "Hydrotropic pretreatment on rice straw for bioethanol production," Renewable Energy, Elsevier, vol. 98(C), pages 2-8.
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    4. Zhao, Chen & Xie, Bing & Zhao, Runze & Fang, Hao, 2019. "Microbial oil production by Mortierella isabellina from sodium hydroxide pretreated rice straw degraded by three-stage enzymatic hydrolysis in the context of on-site cellulase production," Renewable Energy, Elsevier, vol. 130(C), pages 281-289.
    5. Behera, Shuvashish & Arora, Richa & Nandhagopal, N. & Kumar, Sachin, 2014. "Importance of chemical pretreatment for bioconversion of lignocellulosic biomass," Renewable and Sustainable Energy Reviews, Elsevier, vol. 36(C), pages 91-106.
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    2. Nishu, & Li, Chong & Yellezuome, Dominic & Li, Yingkai & Liu, Ronghou, 2023. "Catalytic pyrolysis of rice straw for high yield of aromatics over modified ZSM-5 catalysts and its kinetics," Renewable Energy, Elsevier, vol. 209(C), pages 569-580.
    3. Radhakrishnan, Rokesh & Manna, Bharat & Ghosh, Amit, 2023. "Molecular insights into dissolution of lignin bunch in ionic liquid-water mixture for enhanced biomass conversion," Renewable Energy, Elsevier, vol. 206(C), pages 47-59.

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