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Integration of extraction and transesterification of lipid from jatropha seeds for the production of biodiesel

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  • Lian, Shuang
  • Li, Huijuan
  • Tang, Jinqiang
  • Tong, Dongmei
  • Hu, Changwei

Abstract

A process integrating the extraction and transesterification of lipid from jatropha kernel powder for the production of biodiesel with methanol assisted by hexane is reported in this paper. The effects of catalyst amount, reaction time, reaction temperature, and siphon tube height on the yield and characteristics of biodiesel were investigated. It was found that hexane played the role of both co-solvent and co-extractant, which enhanced the efficiency of lipid extraction and the formation of a single phase containing methanol and lipid, facilitating mass transfer. Therefore, the reaction system had liquid-flow-solid-catalyzed character. The flow velocity of extraction liquor was controlled to fit for the rate of transesterification via controlling the reaction conditions. The products containing 80.2% fatty acid methyl ester (FAME) were obtained and its high heating value was 37.43MJ/kg. In this process, the residue of kernel powder, catalyst and products were simultaneously separated.

Suggested Citation

  • Lian, Shuang & Li, Huijuan & Tang, Jinqiang & Tong, Dongmei & Hu, Changwei, 2012. "Integration of extraction and transesterification of lipid from jatropha seeds for the production of biodiesel," Applied Energy, Elsevier, vol. 98(C), pages 540-547.
    • Handle: RePEc:eee:appene:v:98:y:2012:i:c:p:540-547
    DOI: 10.1016/j.apenergy.2012.04.029
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    2. Noraini, M.Y. & Ong, Hwai Chyuan & Badrul, Mohamed Jan & Chong, W.T., 2014. "A review on potential enzymatic reaction for biofuel production from algae," Renewable and Sustainable Energy Reviews, Elsevier, vol. 39(C), pages 24-34.
    3. Talebian-Kiakalaieh, Amin & Amin, Nor Aishah Saidina & Mazaheri, Hossein, 2013. "A review on novel processes of biodiesel production from waste cooking oil," Applied Energy, Elsevier, vol. 104(C), pages 683-710.
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    5. Janbarari, Seyed Reza & Ahmadian Behrooz, Hesam, 2020. "Optimal and robust synthesis of the biodiesel production process using waste cooking oil from different feedstocks," Energy, Elsevier, vol. 198(C).
    6. Badawy, Tawfik & Mansour, Mohy S. & Daabo, Ahmed M. & Abdel Aziz, Mostafa M. & Othman, Abdelrahman A. & Barsoum, Fady & Basouni, Mohamed & Hussien, Mohamed & Ghareeb, Mourad & Hamza, Mahmoud & Wang, C, 2021. "Selection of second-generation crop for biodiesel extraction and testing its impact with nano additives on diesel engine performance and emissions," Energy, Elsevier, vol. 237(C).
    7. Navarro-Pineda, Freddy S. & Baz-Rodríguez, Sergio A. & Handler, Robert & Sacramento-Rivero, Julio C., 2016. "Advances on the processing of Jatropha curcas towards a whole-crop biorefinery," Renewable and Sustainable Energy Reviews, Elsevier, vol. 54(C), pages 247-269.

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