Multi-Parameter Analysis of Gas Losses Occurring during the Determination of Methane-Bearing Capacity in Hard Coal Beds

The content of natural methane in hard coal seams, called methane-bearing capacity, is the basic parameter that enables the level of methane hazard to be determined in hard coal mines. This parameter is also used to determine the potential quantities of methane that can be collected and used for energy purposes and the amount of its harmful emission to the atmosphere. Direct methods are most often used to determine methane-bearing capacity. An important aspect that has a great influence on the final result of the research is the gas losses generated at the stage of sampling. Under the conditions of the Polish mining industry, the direct drill cuttings method is used to determine the methane-bearing capacity. Gas losses are compensated for in this method with the use of the coefficient 1.12, by which the obtained result is multiplied. In this paper, a multi-parameter analysis of gas loss in the determination of methane-bearing capacity in hard coal seams has been carried out. Several experiments were performed to identify the most important aspects to be taken into account to obtain a correct result. A methane-bearing capacity test was conducted using two direct methods: the direct drill cuttings method, otherwise known as the single-phase vacuum degassing method, and a method based on the United States Bureau of Mines standards. Sorption studies, such as methane sorption kinetics tests, were also conducted in which sorption properties, such as sorption capacity, effective diffusion coefficient, and half sorption time, were determined. Methane sorption isotherms were also determined, and pore structure was analysed. Based on the obtained test results, an analysis was carried out which made it possible to present appropriate conclusions concerning the gas losses during the methane-bearing capacity test, generated at the stage of sampling. The final result of the work was the proposal of a new gas loss coefficient for the direct drill cuttings method of methane-bearing capacity determination.