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Preparation of a supported acidic ionic liquid on silica-gel and its application to the synthesis of biodiesel from waste cooking oil

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  • Cao, Yang
  • Zhou, Houbo
  • Li, Jin

Abstract

An environmental acidic ionic liquid was prepared with 1-allyl-1H-imidazole, 1,3-propyl sulfonic acid lactone and H2SO4 and was immobilized on silica-gel to synthesize the catalyst used to prepare biodiesel from waste cooking oil by a one-step method. The structure of the catalyst was characterized by BET, FTIR, DSC/TGA and SEM. The effect of methanol oil mole ratio, catalyst dosage, reaction temperature, and reaction time on the conversion of waste cooking oil to biodiesel was investigated, and the optimum reaction conditions were determined by an orthogonal test. The optimum reaction conditions were shown as follows: methanol oil mole ratio of 25:1, catalyst dosage of 5wt% of oil, reaction temperature of 60°C, reaction time of 20h, and the yield of 87.58%. The yield could reach 70.02% after reusing the catalyst 5 times.

Suggested Citation

  • Cao, Yang & Zhou, Houbo & Li, Jin, 2016. "Preparation of a supported acidic ionic liquid on silica-gel and its application to the synthesis of biodiesel from waste cooking oil," Renewable and Sustainable Energy Reviews, Elsevier, vol. 58(C), pages 871-875.
    • Handle: RePEc:eee:rensus:v:58:y:2016:i:c:p:871-875
    DOI: 10.1016/j.rser.2015.12.237
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    References listed on IDEAS

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    1. Borges, M.E. & Díaz, L., 2012. "Recent developments on heterogeneous catalysts for biodiesel production by oil esterification and transesterification reactions: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 16(5), pages 2839-2849.
    2. Atadashi, I.M. & Aroua, M.K. & Abdul Aziz, A.R. & Sulaiman, N.M.N., 2012. "The effects of water on biodiesel production and refining technologies: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 16(5), pages 3456-3470.
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    2. Han, Xiaoxiang & Jiang, Shengchou & Chen, Ziyi & Zeng, Zhiwei & Chen, Qing & Niu, Fuge & Pan, Weichun & Tang, Xiujuan & Liu, Shang-Bin, 2023. "Highly active sulfonic ionic liquid modified heteropoly acid composite catalysts for efficient production of ethyl palmitate," Renewable Energy, Elsevier, vol. 215(C).
    3. Dai, Qiqi & Yang, Zifei & Li, Jin & Cao, Yang & Tang, Hongbiao & Wei, Xiaocui, 2021. "Zirconium-based MOFs-loaded ionic liquid-catalyzed preparation of biodiesel from Jatropha oil," Renewable Energy, Elsevier, vol. 163(C), pages 1588-1594.
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    5. Li, Xin & Luo, Xingyi & Jin, Yangbin & Li, Jinyan & Zhang, Hongdan & Zhang, Aiping & Xie, Jun, 2018. "Heterogeneous sulfur-free hydrodeoxygenation catalysts for selectively upgrading the renewable bio-oils to second generation biofuels," Renewable and Sustainable Energy Reviews, Elsevier, vol. 82(P3), pages 3762-3797.

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