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Precipitation recovery of boron from aqueous solution by chemical oxo-precipitation at room temperature

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  • Lin, Jui-Yen
  • Shih, Yu-Jen
  • Chen, Po-Yen
  • Huang, Yao-Hui

Abstract

This work investigated the effective precipitation recovery of boron by chemical oxo-precipitation (COP), which uses hydrogen peroxide (H2O2) to transform aqueous boron to easy-precipitating perborates at room temperature. By using barium hydroxide (Ba(OH)2) as a precipitant, the boron removal enhanced with treatment time and the boron level was eventually reduced from 1000ppm to 3ppm in four hours. The transformation of the precipitates from amorphous to crystalline was assumed to be responsible for such high boron removal. The aqueous data and the characterization of the precipitates, including elemental analysis, dissolved oxygen, XRD and Raman microscopy, reveal that the phase transformation of perborate species in the precipitates carried out with time during the COP. Mechanisms of COP that describe the precipitates transformation from BaB(OH)3OOB(OH)3 and Ba(B(OH)3OOH)2 to BaB(OH)2(OO)2B(OH)2 were proposed.

Suggested Citation

  • Lin, Jui-Yen & Shih, Yu-Jen & Chen, Po-Yen & Huang, Yao-Hui, 2016. "Precipitation recovery of boron from aqueous solution by chemical oxo-precipitation at room temperature," Applied Energy, Elsevier, vol. 164(C), pages 1052-1058.
    • Handle: RePEc:eee:appene:v:164:y:2016:i:c:p:1052-1058
    DOI: 10.1016/j.apenergy.2014.12.058
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    References listed on IDEAS

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    1. Kim, Sung Han & Miesse, Craig M. & Lee, Hee Bum & Chang, Ik Whang & Hwang, Yong Sheen & Jang, Jae Hyuk & Cha, Suk Won, 2014. "Ultra compact direct hydrogen fuel cell prototype using a metal hydride hydrogen storage tank for a mobile phone," Applied Energy, Elsevier, vol. 134(C), pages 382-391.
    2. Sharaf, Omar Z. & Orhan, Mehmet F., 2014. "An overview of fuel cell technology: Fundamentals and applications," Renewable and Sustainable Energy Reviews, Elsevier, vol. 32(C), pages 810-853.
    3. Wang, Yun & Chen, Ken S. & Mishler, Jeffrey & Cho, Sung Chan & Adroher, Xavier Cordobes, 2011. "A review of polymer electrolyte membrane fuel cells: Technology, applications, and needs on fundamental research," Applied Energy, Elsevier, vol. 88(4), pages 981-1007, April.
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    1. Xiaowei Liu & Congjin Xu & Peng Chen & Kexin Li & Qikun Zhou & Miaomaio Ye & Liang Zhang & Ye Lu, 2022. "Advances in Technologies for Boron Removal from Water: A Comprehensive Review," IJERPH, MDPI, vol. 19(17), pages 1-34, August.

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