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A review on the characterization of hydrogen in hydrogen storage materials

Author

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  • Wei, T.Y.
  • Lim, K.L.
  • Tseng, Y.S.
  • Chan, S.L.I.

Abstract

In order to realize a low-carbon hydrogen economy, a continuous search for materials able to store hydrogen in the solid form has been actively carried out globally. The need to accurately characterize the hydrogen storage properties of a variety of materials, including the thermodynamic and kinetic information, is of paramount importance. However owning to the diversity of potential hydrogen storage materials, it is essential to select a proper technique for characterize hydrogen storage properties to avoid faulty results. This paper serves as a critical review on several techniques commonly employed to characterize hydrogen storage materials. In this context, the working principles, advantages and drawbacks, limitations of six categories of techniques – Sieverts method, gravimetric method, secondary ion mass spectrometry, thermal desorption spectroscopy, neutron scattering and electrochemical techniques – are described and reviewed. It can be seen that Sieverts method is a powerful tool for metal hydride samples under normal testing regime. Gravimetric method can be used to investigate the hydrogen storage of porous samples since it normally suffers less from the sample volume uncertainty, however careful buoyancy correction must be applied to avoid faulty results. Secondary ion mass spectroscopy and thermal desorption spectroscopy can be used to study the surface/subsurface hydrogen profile and thermodynamic/kinetic properties of gas desorption of sample, respectively, providing that these samples are stable under vacuum. Neutron scattering is capable of investigating varies types of information including structural, diffusion and hydrogen dynamics of host material under in-stiu environment, although the neutron resources is not always accessible for most researchers. Electrochemical method can be used to study thermodynamic/kinetic properties for both thin film and bulk samples, but it may not be applicable to samples with low corrosion resistance and high plateau pressure.

Suggested Citation

  • Wei, T.Y. & Lim, K.L. & Tseng, Y.S. & Chan, S.L.I., 2017. "A review on the characterization of hydrogen in hydrogen storage materials," Renewable and Sustainable Energy Reviews, Elsevier, vol. 79(C), pages 1122-1133.
    • Handle: RePEc:eee:rensus:v:79:y:2017:i:c:p:1122-1133
    DOI: 10.1016/j.rser.2017.05.132
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    References listed on IDEAS

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    1. Pudukudy, Manoj & Yaakob, Zahira & Mohammad, Masita & Narayanan, Binitha & Sopian, Kamaruzzaman, 2014. "Renewable hydrogen economy in Asia – Opportunities and challenges: An overview," Renewable and Sustainable Energy Reviews, Elsevier, vol. 30(C), pages 743-757.
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    4. Hosseini, Seyed Ehsan & Wahid, Mazlan Abdul, 2016. "Hydrogen production from renewable and sustainable energy resources: Promising green energy carrier for clean development," Renewable and Sustainable Energy Reviews, Elsevier, vol. 57(C), pages 850-866.
    5. Chaubey, Rashmi & Sahu, Satanand & James, Olusola O. & Maity, Sudip, 2013. "A review on development of industrial processes and emerging techniques for production of hydrogen from renewable and sustainable sources," Renewable and Sustainable Energy Reviews, Elsevier, vol. 23(C), pages 443-462.
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    2. Calabrese, M. & Russo, D. & di Benedetto, A. & Marotta, R. & Andreozzi, R., 2023. "Formate/bicarbonate interconversion for safe hydrogen storage: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 173(C).
    3. Zhang, Huaiwei & Bao, Liang & Qi, Jianbo & Xuan, Weidong & Fu, Li & Yuan, Yongjun, 2020. "Effects of nano-molybdenum coatings on the hydrogen storage properties of La–Mg–Ni based alloys," Renewable Energy, Elsevier, vol. 157(C), pages 1053-1060.
    4. Renato Belli Strozi & Daniel Rodrigo Leiva & Guilherme Zepon & Walter José Botta & Jacques Huot, 2021. "Effects of the Chromium Content in (TiVNb) 100−x Cr x Body-Centered Cubic High Entropy Alloys Designed for Hydrogen Storage Applications," Energies, MDPI, vol. 14(11), pages 1-11, May.

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