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Fast Production of High Performance LiNi 0.815 Co 0.15 Al 0.035 O 2 Cathode Material via Urea-Assisted Flame Spray Pyrolysis

Author

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  • Cornelius Satria Yudha

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia
    Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia)

  • Soraya Ulfa Muzayanha

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia
    Research & Technology Centre, PT. Pertamina (Persero), Jl. Raya Bekas Km 20, Pulogadung, Jakarta 19320, Indonesia)

  • Mintarsih Rahmawati

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia
    Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia)

  • Hendri Widiyandari

    (Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia
    Department of Physics, Faculty of Mathematic and Natural Science, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia)

  • Wahyudi Sutopo

    (Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia
    Department of Industrial Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia)

  • Muhammad Nizam

    (Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia
    Department of Electrical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia)

  • Sigit Puji Santosa

    (National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia
    Department of Mechanical Engineering, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia)

  • Agus Purwanto

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta 57126, Indonesia
    Lithium Battery Research and Technology Centre, Universitas Sebelas Maret, Jl. Slamet Riyadi 435, Surakarta 57146, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung 40132, Indonesia)

Abstract

The high throughput and rapid flame-assisted spray pyrolysis method has been adapted to synthesize cathode materials LiNi 0.ap Co 0.15 Al 0.035 O 2 (NCA). This method is considered low cost and simple. By varying the precursor solution concentration and sintering temperature, the optimal condition was established at temperature sintering of 800 °C and precursor solution concentration of 1 M. X-ray diffraction patterns showed the as-prepared NCA particles exhibit a pure well-ordered hexagonal layer structure with high crystallinity. Polyhedral shaped micro-sized particles are confirmed by SEM images. Galvanostic charge–discharge tests were conducted using cylindrical full-cell utilizing artificial graphite as the anode. The highest specific initial discharge capacity measured between 2.7 and 4.3 V is 155 mAh g −1 with capacity retention of 92% after cycled at 0.2 C for 50 cycles. Thus, this method is considered as a satisfying approach for NCA mass production.

Suggested Citation

  • Cornelius Satria Yudha & Soraya Ulfa Muzayanha & Mintarsih Rahmawati & Hendri Widiyandari & Wahyudi Sutopo & Muhammad Nizam & Sigit Puji Santosa & Agus Purwanto, 2020. "Fast Production of High Performance LiNi 0.815 Co 0.15 Al 0.035 O 2 Cathode Material via Urea-Assisted Flame Spray Pyrolysis," Energies, MDPI, vol. 13(11), pages 1-17, June.
    • Handle: RePEc:gam:jeners:v:13:y:2020:i:11:p:2757-:d:365602
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    References listed on IDEAS

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    1. Linjing Zhang & Jiuchun Jiang & Weige Zhang, 2017. "Capacity Decay Mechanism of the LCO + NMC532/Graphite Cells Combined with Post-Mortem Technique," Energies, MDPI, vol. 10(8), pages 1-16, August.
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    Cited by:

    1. Cornelius Satria Yudha & Anjas Prasetya Hutama & Mintarsih Rahmawati & Hendri Widiyandari & Hartoto Nursukatmo & Hanida Nilasary & Haryo Satriya Oktaviano & Agus Purwanto, 2021. "Synthesis and Characterization of ZnO from Thermal Decomposition of Precipitated Zinc Oxalate Dihydrate as an Anode Material of Li-Ion Batteries," Energies, MDPI, vol. 14(18), pages 1-13, September.

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