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Efficient conversion of glucose into 5-HMF catalyzed by lignin-derived mesoporous carbon solid acid in a biphasic system

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  • Wang, Shuai
  • Eberhardt, Thomas L.
  • Guo, Dayi
  • Feng, Junfeng
  • Pan, Hui

Abstract

A lignin-derived mesoporous carbon solid acid (LDMCS) catalyst was prepared by high temperature carbonization and subsequent sulfonation treatment using alkali lignin as the carbon source and KCl as a salt template. The prepared LDMCS has an irregular mesoporous structure with a narrow pore size distribution (concentrated at 4 nm), large specific surface area (1123.0 m2 g−1) and high -SO3H group density (2.20 mmol g−1). Compared with other types of solid acids reported in the literature, the prepared LDMCS catalyst has equivalent or better catalytic performance in the catalytic conversion of glucose to 5-hydroxymethylfurfural (5-HMF). A glucose conversion of 97.7% and a 5-HMF yield of 57.8% were obtained with the aqNaCl-THF (1:3) biphasic solvent system under the optimized reaction conditions with reaction temperature of 160 °C, reaction time of 2.5 h, and catalyst loading of 1 mg mg−1. More importantly, the 5-HMF yield still reached 40.9% after 5 cycles of the catalyst use, indicating that there was no significant loss of catalytic activity.

Suggested Citation

  • Wang, Shuai & Eberhardt, Thomas L. & Guo, Dayi & Feng, Junfeng & Pan, Hui, 2022. "Efficient conversion of glucose into 5-HMF catalyzed by lignin-derived mesoporous carbon solid acid in a biphasic system," Renewable Energy, Elsevier, vol. 190(C), pages 1-10.
    • Handle: RePEc:eee:renene:v:190:y:2022:i:c:p:1-10
    DOI: 10.1016/j.renene.2022.03.021
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    References listed on IDEAS

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    1. Karimi, Sabah & Seidi, Farzad & Niakan, Mahsa & Shekaari, Hemayat & Masteri-Farahani, Majid, 2021. "Catalytic dehydration of fructose into 5-hydroxymethylfurfural by propyl sulfonic acid functionalized magnetic graphene oxide nanocomposite," Renewable Energy, Elsevier, vol. 180(C), pages 132-139.
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    1. Niakan, Mahsa & Masteri-Farahani, Majid & Seidi, Farzad, 2022. "Efficient glucose-to-HMF conversion in deep eutectic solvents over sulfonated dendrimer modified activated carbon," Renewable Energy, Elsevier, vol. 200(C), pages 1134-1140.
    2. Cai, Bo & Kang, Rui & Guo, Dayi & Feng, Junfeng & Ma, Tianyi & Pan, Hui, 2022. "An eco-friendly acidic catalyst phosphorus-doped graphitic carbon nitride for efficient conversion of fructose to 5-Hydroxymethylfurfural," Renewable Energy, Elsevier, vol. 199(C), pages 1629-1638.
    3. Zhao, Xiaolan & Gao, Pei & Shen, Boxiong & Wang, Xiaoqi & Yue, Tian & Han, Zhibin, 2023. "Recent advances in lignin-derived mesoporous carbon based-on template methods," Renewable and Sustainable Energy Reviews, Elsevier, vol. 188(C).

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