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Colloidal processing and CO2 capture performance of sacrificially templated zeolite monoliths

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  • Akhtar, Farid
  • Andersson, Linnéa
  • Keshavarzi, Neda
  • Bergström, Lennart

Abstract

Sacrificial templating of suspension cast and subsequently thermally treated zeolite monoliths with glassy carbon spheres and fibers yielded zeolite 13X and silicalite-1 monoliths with macroporosities up to 50vol%. Homogeneous distribution of the macroporosity in hierarchically porous monoliths was obtained by tailoring the surface chemistry of the carbon particles by polyelectrolyte-assisted adsorption of zeolite particles. The effect of amount of kaolin binder and temperature for the thermal treatment on the monoliths strength, surface area and CO2 uptake was studied by diametral compression tests, electron microscopy, X-ray diffraction and gas adsorption. Cyclic adsorption and regeneration measurements showed that zeolite 13X monoliths display a high CO2 uptake while the silicalite-1 monoliths could be regenerated with a relatively low energy penalty.

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  • Akhtar, Farid & Andersson, Linnéa & Keshavarzi, Neda & Bergström, Lennart, 2012. "Colloidal processing and CO2 capture performance of sacrificially templated zeolite monoliths," Applied Energy, Elsevier, vol. 97(C), pages 289-296.
    • Handle: RePEc:eee:appene:v:97:y:2012:i:c:p:289-296
    DOI: 10.1016/j.apenergy.2011.12.064
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    1. Zhao, Guoying & Aziz, Baroz & Hedin, Niklas, 2010. "Carbon dioxide adsorption on mesoporous silica surfaces containing amine-like motifs," Applied Energy, Elsevier, vol. 87(9), pages 2907-2913, September.
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    2. Li, Kaimin & Jiang, Jianguo & Yan, Feng & Tian, Sicong & Chen, Xuejing, 2014. "The influence of polyethyleneimine type and molecular weight on the CO2 capture performance of PEI-nano silica adsorbents," Applied Energy, Elsevier, vol. 136(C), pages 750-755.
    3. Qasem, Naef A.A. & Ben-Mansour, Rached, 2018. "Energy and productivity efficient vacuum pressure swing adsorption process to separate CO2 from CO2/N2 mixture using Mg-MOF-74: A CFD simulation," Applied Energy, Elsevier, vol. 209(C), pages 190-202.
    4. Li, Bingyun & Duan, Yuhua & Luebke, David & Morreale, Bryan, 2013. "Advances in CO2 capture technology: A patent review," Applied Energy, Elsevier, vol. 102(C), pages 1439-1447.
    5. Hedin, Niklas & Andersson, Linnéa & Bergström, Lennart & Yan, Jinyue, 2013. "Adsorbents for the post-combustion capture of CO2 using rapid temperature swing or vacuum swing adsorption," Applied Energy, Elsevier, vol. 104(C), pages 418-433.
    6. Myat, Aung & Kim Choon, Ng & Thu, Kyaw & Kim, Young-Deuk, 2013. "Experimental investigation on the optimal performance of Zeolite–water adsorption chiller," Applied Energy, Elsevier, vol. 102(C), pages 582-590.
    7. Ganapathy, Harish & Steinmayer, Sascha & Shooshtari, Amir & Dessiatoun, Serguei & Ohadi, Michael M. & Alshehhi, Mohamed, 2016. "Process intensification characteristics of a microreactor absorber for enhanced CO2 capture," Applied Energy, Elsevier, vol. 162(C), pages 416-427.
    8. Su, Fengsheng & Lu, Chungsying & Chung, Ai-Ju & Liao, Chien-Hsiang, 2014. "CO2 capture with amine-loaded carbon nanotubes via a dual-column temperature/vacuum swing adsorption," Applied Energy, Elsevier, vol. 113(C), pages 706-712.
    9. Ganapathy, H. & Shooshtari, A. & Dessiatoun, S. & Alshehhi, M. & Ohadi, M., 2014. "Fluid flow and mass transfer characteristics of enhanced CO2 capture in a minichannel reactor," Applied Energy, Elsevier, vol. 119(C), pages 43-56.
    10. Chao, Cong & Deng, Yimin & Dewil, Raf & Baeyens, Jan & Fan, Xianfeng, 2021. "Post-combustion carbon capture," Renewable and Sustainable Energy Reviews, Elsevier, vol. 138(C).
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