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Preliminary evaluation of organosolv pre-treatment of sugar cane bagasse for glucose production: Application of 23 experimental design

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  • Mesa, Leyanis
  • González, Erenio
  • Ruiz, Encarnación
  • Romero, Inmaculada
  • Cara, Cristóbal
  • Felissia, Fernando
  • Castro, Eulogio

Abstract

Sugar cane bagasse was submitted to ethanol organosolv pre-treatment using a 50 L pilot scale reactor. The influence of catalyst type (H2SO4 or NaOH), catalyst concentration (1.25-1.50% w/w on dry fiber) and process time (60-90 min) on total solid recovery and solid composition (glucan, xylan and lignin contents) was evaluated by performing a 23 full factorial experimental design. Pretreated sugar cane bagasse was further submitted to enzymatic hydrolysis using a commercial enzyme complex formed by cellulases and [beta]-glucosidases. Glucose concentration in the hydrolysates and glucose yield referred to initial raw material (g glucose/100 g sugar cane bagasse) were used to select the best operational conditions. Concerning the enzymatic hydrolysis, the resulting glucose concentration was found to be dependent on xylan contents of the pretreated material. The modelling equations for glucose concentration and glucose yield as a function of the pre-treatment variables and the statistical analysis are also discussed in this work.

Suggested Citation

  • Mesa, Leyanis & González, Erenio & Ruiz, Encarnación & Romero, Inmaculada & Cara, Cristóbal & Felissia, Fernando & Castro, Eulogio, 2010. "Preliminary evaluation of organosolv pre-treatment of sugar cane bagasse for glucose production: Application of 23 experimental design," Applied Energy, Elsevier, vol. 87(1), pages 109-114, January.
    • Handle: RePEc:eee:appene:v:87:y:2010:i:1:p:109-114
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    References listed on IDEAS

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    3. Ruiz, Héctor A. & Rodríguez-Jasso, Rosa M. & Fernandes, Bruno D. & Vicente, António A. & Teixeira, José A., 2013. "Hydrothermal processing, as an alternative for upgrading agriculture residues and marine biomass according to the biorefinery concept: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 21(C), pages 35-51.
    4. Cybulska, Iwona & Brudecki, Grzegorz P. & Zembrzuska, Joanna & Schmidt, Jens Ejbye & Lopez, Celia Garcia-Banos & Thomsen, Mette Hedegaard, 2017. "Organosolv delignification of agricultural residues (date palm fronds, Phoenix dactylifera L.) of the United Arab Emirates," Applied Energy, Elsevier, vol. 185(P2), pages 1040-1050.
    5. Mesa, Leyanis & López, Nancy & Cara, Cristóbal & Castro, Eulogio & González, Erenio & Mussatto, Solange I., 2016. "Techno-economic evaluation of strategies based on two steps organosolv pretreatment and enzymatic hydrolysis of sugarcane bagasse for ethanol production," Renewable Energy, Elsevier, vol. 86(C), pages 270-279.
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    7. Caspeta, Luis & Caro-Bermúdez, Mario A. & Ponce-Noyola, Teresa & Martinez, Alfredo, 2014. "Enzymatic hydrolysis at high-solids loadings for the conversion of agave bagasse to fuel ethanol," Applied Energy, Elsevier, vol. 113(C), pages 277-286.
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