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Synthesized “In Situ” In Reverse Micelles Of Silver-Sulfide Semiconductors

Author

Listed:
  • M.P. PILENI

    (Université P. et M. Curie, Laboratoire SRSI, BP 52, Bat 74, 4 place Jussieu, 75005 Paris, France;
    CEN Saclay, DRECAM-SCM, Bat 522, 91191 Gif sur Yvette, France;)

  • L. MOTTE

    (Université P. et M. Curie, Laboratoire SRSI, BP 52, Bat 74, 4 place Jussieu, 75005 Paris, France;
    CEN Saclay, DRECAM-SCM, Bat 522, 91191 Gif sur Yvette, France)

  • F. BILLOUDET

    (Université P. et M. Curie, Laboratoire SRSI, BP 52, Bat 74, 4 place Jussieu, 75005 Paris, France)

  • C. PETIT

    (Université P. et M. Curie, Laboratoire SRSI, BP 52, Bat 74, 4 place Jussieu, 75005 Paris, France;
    CEN Saclay, DRECAM-SCM, Bat 522, 91191 Gif sur Yvette, France)

Abstract

Functionalized reverse micelles are used to control the size of silver sulfide,Ag2S, nanosize particles. The size of the crystallites varies linearly with the water content from 2 to 10 nm. The particles have been coated with dodecanethiol and extracted from micelles. The size of the particles dispersed in heptane has been determined by small-angles x-ray scattering (SAXS) experiments and compared to those obtained by transmission electron microscopy (TEM). A good agreement between results is obtained by these two techniques. A drop of particles previously dispersed in heptane is dried on a carbon grill. A network of the particles forming monolayers of crystallites in a hexagonal distribution appears.

Suggested Citation

  • M.P. Pileni & L. Motte & F. Billoudet & C. Petit, 1996. "Synthesized “In Situ” In Reverse Micelles Of Silver-Sulfide Semiconductors," Surface Review and Letters (SRL), World Scientific Publishing Co. Pte. Ltd., vol. 3(01), pages 1215-1218.
    • Handle: RePEc:wsi:srlxxx:v:03:y:1996:i:01:n:s0218625x96002199
    DOI: 10.1142/S0218625X96002199
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