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Preparation and performance investigation of a lignin-based solid acid catalyst manufactured from olive cake for biodiesel production

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  • Sandouqa, Arwa
  • Al-Hamamre, Zayed
  • Asfar, Jamil

Abstract

In this study, the olive cake was successfully developed and applied as a substrate to produce a lignin-based catalyst for biodiesel production. Three lignin-based solid acid catalysts were prepared from the incomplete carbonized alkali lignin using concentrated sulfuric acid. The catalyst underwent a detailed characterization analysis in terms of its functional groups of active sites, surface area, acid sites density and morphological structure. For the catalytic activity test, prepared catalysts were studied for their ability to catalyze both esterification and transesterification reactions of waste vegetable oil (WVO) ≈2 FFA (% w/w).

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  • Sandouqa, Arwa & Al-Hamamre, Zayed & Asfar, Jamil, 2019. "Preparation and performance investigation of a lignin-based solid acid catalyst manufactured from olive cake for biodiesel production," Renewable Energy, Elsevier, vol. 132(C), pages 667-682.
    • Handle: RePEc:eee:renene:v:132:y:2019:i:c:p:667-682
    DOI: 10.1016/j.renene.2018.08.029
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    Cited by:

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    5. Mohammad Alnaief & Arwa Sandouqa & Ibrahem Altarawneh & Mohammad Al-Shannag & Malek Alkasrawi & Zayed Al-hamamre, 2020. "Adsorption Characteristics and Potential of Olive Cake Alkali Residues for Biodiesel Purification," Energies, MDPI, vol. 14(1), pages 1-12, December.
    6. Rokhum, Samuel Lalthazuala & Changmai, Bishwajit & Kress, Thomas & Wheatley, Andrew E.H., 2022. "A one-pot route to tunable sugar-derived sulfonated carbon catalysts for sustainable production of biodiesel by fatty acid esterification," Renewable Energy, Elsevier, vol. 184(C), pages 908-919.
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    8. Zhang, Bingxin & Gao, Ming & Geng, Jiayu & Cheng, Yuwei & Wang, Xiaona & Wu, Chuanfu & Wang, Qunhui & Liu, Shu & Cheung, Siu Ming, 2021. "Catalytic performance and deactivation mechanism of a one-step sulfonated carbon-based solid-acid catalyst in an esterification reaction," Renewable Energy, Elsevier, vol. 164(C), pages 824-832.
    9. Al-Hamamre, Zayed & Sandouqa, Arwa & Al-Saida, Basel & Shawabkeh, Reyad A. & Alnaief, Mohammad, 2023. "Biodiesel production from waste cooking oil using heterogeneous KNO3/Oil shale ash catalyst," Renewable Energy, Elsevier, vol. 211(C), pages 470-483.
    10. Leesing, Ratanaporn & Siwina, Siraprapha & Fiala, Khanittha, 2021. "Yeast-based biodiesel production using sulfonated carbon-based solid acid catalyst by an integrated biorefinery of durian peel waste," Renewable Energy, Elsevier, vol. 171(C), pages 647-657.
    11. Zhang, Bingxin & Gao, Ming & Tang, Weiqi & Wang, Xiaona & Wu, Chuanfu & Wang, Qunhui & Cheung, Siu Ming & Chen, Xiankun, 2023. "Esterification efficiency improvement of carbon-based solid acid catalysts induced by biomass pretreatments: Intrinsic mechanism," Energy, Elsevier, vol. 263(PB).
    12. Che Zhao & Hongyuan Chen & Xiao Wu & Rui Shan, 2023. "Exploiting the Waste Biomass of Durian Shell as a Heterogeneous Catalyst for Biodiesel Production at Room Temperature," IJERPH, MDPI, vol. 20(3), pages 1-10, January.
    13. Aisien, Felix Aibuedefe & Aisien, Eki Tina, 2023. "Modeling and optimization of transesterification of rubber seed oil using sulfonated CaO derived from giant African land snail (Achatina fulica) catalyst by response surface methodology," Renewable Energy, Elsevier, vol. 207(C), pages 137-146.
    14. Alaei, Shervin & Haghighi, Mohammad & Rahmanivahid, Behgam & Shokrani, Reza & Naghavi, Hossein, 2020. "Conventional vs. hybrid methods for dispersion of MgO over magnetic Mg–Fe mixed oxides nanocatalyst in biofuel production from vegetable oil," Renewable Energy, Elsevier, vol. 154(C), pages 1188-1203.

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