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Preparation of porous carbon materials from biomass pyrolysis vapors for hydrogen storage

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  • Zhang, Huiyan
  • Zhu, Yiwen
  • Liu, Qingyu
  • Li, Xiaowen

Abstract

A novel method for preparing porous carbon materials from biomass pyrolysis vapors with calcium citrate template has been proposed. The effects of pyrolysis temperature, pyrolysis heating rate and carbon-containing precursor preparation temperature on the yield of biomass pyrolysis products, composition of light bio-oil and structure of porous carbons were investigated. The physicochemical characterization and hydrogen adsorption experiments were carried out for the prepared porous carbons. The carbonization mechanism of the carbon-containing precursor was studied and a five-stage reaction kinetic model was established by Gaussian peak separation method according to the DTG curves. Under the optimal conditions of pyrolysis temperature (823 K), heating rate (10 K/min) and carbon-containing precursor preparation temperature (473 K), the prepared porous carbon material has the largest specific surface area of 1703 m2/g, relatively high micropore volume of 0.51 cm3/g and microporosity of 24.17%. The hydrogen adsorption capacity of the carbon material can reach 170.12 cm3/g (1.53 wt%) at 77 K at atmospheric pressure. This paper provides a novel and environmental-friendly method for the preparation of porous carbon materials, and also presents a new way for the utilization of biomass pyrolysis vapors before condensation.

Suggested Citation

  • Zhang, Huiyan & Zhu, Yiwen & Liu, Qingyu & Li, Xiaowen, 2022. "Preparation of porous carbon materials from biomass pyrolysis vapors for hydrogen storage," Applied Energy, Elsevier, vol. 306(PB).
    • Handle: RePEc:eee:appene:v:306:y:2022:i:pb:s0306261921014082
    DOI: 10.1016/j.apenergy.2021.118131
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    References listed on IDEAS

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    1. Trubetskaya, Anna & Timko, Michael T & Umeki, Kentaro, 2020. "Prediction of fast pyrolysis products yields using lignocellulosic compounds and ash contents," Applied Energy, Elsevier, vol. 257(C).
    2. Wang, Chu & Ding, Haozhi & Zhang, Yiming & Zhu, Xifeng, 2020. "Analysis of property variation and stability on the aging of bio-oil from fractional condensation," Renewable Energy, Elsevier, vol. 148(C), pages 720-728.
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    1. Wu, Kai & Yang, Ke & Zhu, Yiwen & Luo, Bingbing & Chu, Chenyang & Li, Mingfan & Zhang, Yuanjian & Zhang, Huiyan, 2023. "The co-pyrolysis interactionsof isolated lignins and cellulose by experiments and theoretical calculations," Energy, Elsevier, vol. 263(PC).
    2. Fuquan Song & Lintao Huang & Heying Ding & Shiming Zhang & Jinbiao Yu, 2023. "In Situ Ni-Doped Hierarchically Porous Carbon Nanofibers Derived from Polyacrylonitrile/Pitch for Hydrogen Storage at Ambient Temperature," Sustainability, MDPI, vol. 15(11), pages 1-13, May.
    3. Wang, Jia & Jiang, Jianchun & Li, Dongxian & Meng, Xianzhi & Zhan, Guowu & Wang, Yunpu & Zhang, Aihua & Sun, Yunjuan & Ruan, Roger & Ragauskas, Arthur J., 2022. "Creating values from wastes: Producing biofuels from waste cooking oil via a tandem vapor-phase hydrotreating process," Applied Energy, Elsevier, vol. 323(C).

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