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Direct production of hexyl levulinate as a potential fuel additive from glucose catalyzed by modified dendritic fibrous nanosilica

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  • Mohammadbagheri, Zahra
  • Najafi Chermahini, Alireza

Abstract

Ultrasonic as a fast and powerful method was applied to prepare dendritic fibrous nanosilica (DFNSU) and the properties of this silica were compared with those of DFNS prepared by hydrothermal method (DFNSH). Using this support, a series of the Zn/DFNSU catalysts were prepared by incorporation of different zinc values using the co-condensation technique. The prepared catalysts were characterized by various methods (FT-IR, XRD, ICP, SEM, TEM, BET, and Py-FT-IR) and applied for direct production of hexyl levulinate from glucose. Among these catalysts, 40Zn/DFNSU exhibited the best results for the production of hexyl levulinate with 55.2% yield under optimum reaction conditions (0.05 g catalyst, 0.07 g glucose, reaction temperature of 200 °C and reaction time of 5 h). Also, the catalytic performance of Zn/DFNSH catalysts with different zinc values was studied under optimum reaction conditions and the maximum yield of hexyl levulinate was 59.2% in the presence of 40Zn/DFNSH catalyst.

Suggested Citation

  • Mohammadbagheri, Zahra & Najafi Chermahini, Alireza, 2020. "Direct production of hexyl levulinate as a potential fuel additive from glucose catalyzed by modified dendritic fibrous nanosilica," Renewable Energy, Elsevier, vol. 147(P1), pages 2229-2237.
    • Handle: RePEc:eee:renene:v:147:y:2020:i:p1:p:2229-2237
    DOI: 10.1016/j.renene.2019.10.031
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    References listed on IDEAS

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    1. Liu, Jie & Wang, Xue-Qian & Yang, Bei-Bei & Liu, Chun-Ling & Xu, Chun-Li & Dong, Wen-Sheng, 2018. "Highly efficient conversion of glucose into methyl levulinate catalyzed by tin-exchanged montmorillonite," Renewable Energy, Elsevier, vol. 120(C), pages 231-240.
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    Cited by:

    1. Oprescu, Elena-Emilia & Enascuta, Cristina-Emanuela & Doukeh, Rami & Calin, Catalina & Lavric, Vasile, 2021. "Characterizing and using a new bi-functional catalyst to sustainably synthesize methyl levulinate from biomass carbohydrates," Renewable Energy, Elsevier, vol. 176(C), pages 651-662.
    2. Tang, Yiwei & Liu, Xiaoning & Xi, Ran & Liu, Le & Qi, Xinhua, 2022. "Catalytic one-pot conversion of biomass-derived furfural to ethyl levulinate over bifunctional Nb/Ni@OMC," Renewable Energy, Elsevier, vol. 200(C), pages 821-831.
    3. Dookheh, Maryam & Najafi Chermahini, Alireza & Saraji, Mohammad, 2022. "Organic-inorganic bi-functionalized hybrid KIT-5: A toolbox for catalytic dehydration of xylose to n-hexyl levulinate," Renewable Energy, Elsevier, vol. 200(C), pages 527-536.

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    1. Tang, Yiwei & Liu, Xiaoning & Xi, Ran & Liu, Le & Qi, Xinhua, 2022. "Catalytic one-pot conversion of biomass-derived furfural to ethyl levulinate over bifunctional Nb/Ni@OMC," Renewable Energy, Elsevier, vol. 200(C), pages 821-831.
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