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Enhanced methanol recovery and glycerol separation in biodiesel production – DWC makes it happen

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  • Kiss, Anton A.
  • Ignat, Radu M.

Abstract

Biodiesel is a renewable fuel that consists of fatty acids methyl esters – currently produced by trans-esterification of glycerides with methanol. After the biodiesel synthesis, the downstream processing steps involve the purification of crude glycerol, as well as the separation of excess methanol (recyclable), glycerol by-product and water (from washing and pre-treatment steps). The separation of the ternary mixture methanol–water–glycerol is carried out in a conventional direct sequence that requires two distillation columns and rather high amounts of energy.

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  • Kiss, Anton A. & Ignat, Radu M., 2012. "Enhanced methanol recovery and glycerol separation in biodiesel production – DWC makes it happen," Applied Energy, Elsevier, vol. 99(C), pages 146-153.
    • Handle: RePEc:eee:appene:v:99:y:2012:i:c:p:146-153
    DOI: 10.1016/j.apenergy.2012.04.019
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    References listed on IDEAS

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    Cited by:

    1. Kiss, Anton A. & Flores Landaeta, Servando J. & Infante Ferreira, Carlos A., 2012. "Towards energy efficient distillation technologies – Making the right choice," Energy, Elsevier, vol. 47(1), pages 531-542.
    2. Long, Nguyen Van Duc & Minh, Le Quang & Nhien, Le Cao & Lee, Moonyong, 2015. "A novel self-heat recuperative dividing wall column to maximize energy efficiency and column throughput in retrofitting and debottlenecking of a side stream column," Applied Energy, Elsevier, vol. 159(C), pages 28-38.
    3. de Raad, Brendon & van Lieshout, Marit & Stougie, Lydia & Ramirez, Andrea, 2023. "Exploring impacts of deployment sequences of industrial mitigation measures on their combined CO2 reduction potential," Energy, Elsevier, vol. 262(PB).
    4. Abel Rodrigues & João Carlos Bordado & Rui Galhano dos Santos, 2017. "Upgrading the Glycerol from Biodiesel Production as a Source of Energy Carriers and Chemicals—A Technological Review for Three Chemical Pathways," Energies, MDPI, vol. 10(11), pages 1-36, November.
    5. Luis, P. & Amelio, A. & Vreysen, S. & Calabro, V. & Van der Bruggen, B., 2014. "Simulation and environmental evaluation of process design: Distillation vs. hybrid distillation–pervaporation for methanol/tetrahydrofuran separation," Applied Energy, Elsevier, vol. 113(C), pages 565-575.

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